毛细管电泳法分离测定食品中山梨酸、苯甲酸、糖精

采用毛细管电泳-紫外检测法，考察了波长，电压，缓冲试剂、浓度、pH对山梨酸、苯甲酸、糖精分离的影响，得到了优化的实验条件．以硼砂20mmol／L(pH=7．5)为运行缓冲溶液．20kV为分离电压，检测波长为230nm的电泳条件下，进样时间为10s，山梨酸、苯甲酸、糖精可在12min内实现分离．山梨酸在5mg／L～50mg／L，苯甲酸在5mg／L～50mg／L，糖精在15mg／L～150mg／L范围内呈良好线性关系，迁移速度、峰面积相对标准偏差均小于4．5％，(n=5)．用上述方法对实际样品进行测定，回收率在95％以上．     

正丁烷氧化制顺酐钒磷氧催化剂的助催化作用及活性评价

通过有机相中还原五价钒制得钒磷氧催化荆前驱体，然后用漫渍法引入具有与V^4 离子半径相近的Fe、Co、Cu元素，并完成了正丁烷选择氧化制顺丁烯二酸酐的固定床活性评价试验，探讨了助荆对催化荆性能的影响以及反应条件、活性相结构对顺酐收率的影响．实验结果表明．加入助荆可提高催化荆活性和顺酐收率。复合组分的催化性能优于单一组分，适宜的反应条件是提高顺酐收率的前提，活性相(VO)2RO7(O20)晶面适宜失序对提高顺酐收率具有重要作用．     

兽药添加剂喹乙醇对水生生物的毒理学研究

兽药添加剂喹乙醇是一种在畜禽及水产养殖中应用广泛的促生长剂 ,但其安全性仍存在较大争议 ,使用不当或过量使用会对环境构成潜在危害 .采用斑马鱼和鲤鱼作为生物材料 ,分别研究了兽药添加剂喹乙醇对斑马鱼的急性毒性、对斑马鱼胚胎发育的影响及对鲤鱼肾细胞DNA的损伤 .急性毒性试验表明 ,96hrLC50 为 1 996.87mg/L ;胚胎发育试验实验结果表明 ,96hrEC50 为2 2 1 .2 0mg/L ;单细胞凝胶电泳试验结果表明 ,喹乙醇能引起较大的DNA损伤 ,与空白对照相比有极显著性差异 (P <0 .0 1) ,并在设定的剂量范围内呈现一定的剂量效应关系     

Treed Avalanche Forecasting: Mitigating Avalanche Danger Utilizing Bayesian Additive Regression Trees

Little Cottonwood Canyon Highway is a dead‐end, two‐lane road leading to Utah's Alta and Snowbird ski resorts. It is the only road access to these resorts and is heavily traveled during the ski season. Professional avalanche forecasters monitor this road throughout the ski season in order to make road closure decisions in the face of avalanche danger. Forecasters at the Utah Department of Transportation (UDOT) avalanche guard station at Alta have maintained an extensive daily winter database on explanatory variables relating to avalanche prediction. Whether or not an avalanche crosses the road is modeled in this paper via Bayesian additive tree methods. Utilizing daily winter data from 1995 to 2011, results show that using Bayesian tree analysis outperforms traditional statistical methods in terms of realized misclassification costs that take into consideration asymmetric losses arising from two types of error. Closing the road when an avalanche does not occur is an error harmful to resort owners, and not closing the road when one does may result in injury or death. Copyright © 2016 John Wiley & Sons, Ltd.     

带有加性噪声的阻尼吊桥方程随机吸引子的存在性

用算子分解技巧, 通过对方程的解进行先验估计, 给出随机动力系统的一致渐近紧性, 从而证明了随机吊桥方程在加性噪声下随机吸引子的存在性.     

The total cost of misclassification in credit scoring: A comparison of generalized linear models and generalized additive models

This study examines whether the evaluation of a bankruptcy prediction model should take into account the total cost of misclassification. For this purpose, we introduce and apply a validity measure in credit scoring that is based on the total cost of misclassification. Specifically, we use comprehensive data from the annual financial statements of a sample of German companies and analyze the total cost of misclassification by comparing a generalized linear model and a generalized additive model with regard to their ability to predict a company's probability of default. On the basis of these data, the validity measure we introduce shows that, compared to generalized linear models, generalized additive models can reduce substantially the extent of misclassification and the total cost that this entails. The validity measure we introduce is informative and justifies the argument that generalized additive models should be preferred, although such models are more complex than generalized linear models. We conclude that to balance a model's validity and complexity, it is necessary to take into account the total cost of misclassification.     

电喷汽油机燃用大比例含水乙醇汽油的试验

在一台JL368Q双燃料多点电喷发动机上进行台架试验,对比分析了3种含水乙醇汽油(E15W、E30W、E50W)的动力性、经济性和排放特性.结果表明:在汽油机结构及参数未做任何调整下,低速时,含水乙醇汽油的转距、功率和93#汽油基本相当,随着转速增大,E15W、E50W略低于93#汽油,E30W仍和汽油基本相当;油耗率E15W比汽油低大约0.35%,随着含醇量的增大,油耗率逐渐升高;3种乙醇汽油的NOx排放均略高于93#汽油,但CO的排放都低于93#汽油,E30W的CO排放在整个测试区间最优.随着含醇量的增加,HC排放能得到不断的改善.     

关于r次可加补数的一些复合函数的均值性质

运用初等方法,研究了关于正整数n的r次可加补数函数ar(n)与一些数论函数的复合函数的均值问题,给出了相应函数均值估计的渐近公式.     

2-模和R-2-模的关系

在范畴化理论的基础上,利用预见性范畴和可加2-函子的性质,证明了2-模和R-2模之间的关系,从而得到其相关理论的对应关系,并拓展进一步研究和应用2-模理论,对研究高维同调代数理论有重要作用.     

复合外加剂在道路工程水泥中的应用

将三种不同配方的复合外加剂:掺加萘系(Ⅰ)、掺加氨基磺酸盐(Ⅱ)和萘系+氨基磺酸盐(Ⅲ)按不同掺量加入到水泥中,比较测出的水泥净浆流动度和水泥砂浆抗折、抗压强度,选出一种使水泥净浆流动度经时损失较小、水泥砂浆强度高、压折比较小的方案.结果表明:掺加萘系+氨基磺酸盐(Ⅲ)复合外加剂是符合公路工程要求的一种优化方案.