6-异丙基-3-甲酰基色酮双杂环衍生物的合成

以6-异丙基-3-甲酰基色酮为原料分别与胺、3-乙酰基香豆素以及乙酰甘氨酸反应,得到了5个未见报道的含3-杂环取代的色酮或色满酮类双杂环化合物,产率46%~73%。通过元素分析、MS、IR、1H NMR对其结构进行了确认。同时用X射线单晶衍射法测定了2-乙氧基-6-异丙基-3-(吗啉亚甲基)-4-色酮的晶体结构,晶体属单斜晶系,P21/n空间群,晶胞参数为:a=1.338 5(3)nm,b=0.868 38(17)nm,c=1.668 4(3)nm,β=108.59(3)°,V=1.838 0(6)nm3,Z=4,Dx=1.190 Mg/m3,μ=0.079 mm-1,F(000)=712,R=0.069 2,wR=0.138 7。     

基于PLC的温度控制在电镀生产线中的应用

介绍了以三菱FX0NPLC为核心的温度控制系统在电镀生产线中的应用。简述了温度控制原理,论述了控制系统的设计方案及其软硬件的实现方法。实践表明该方法简单易行,适应性好,可靠性高。     

微机排版校对中易出现的差错及对策

从多方面分析了排版校对过程中容易产生的差错，并从编辑应具备的计算机素养、排版软件所具有的功能及校对技巧出发，提出了如何防止这类差错发生的具体措施．     

辽宁男排跳发球技术分析

跳发球是现代排球比赛中一项攻击力很强的发球技术,为当今世界强队所广泛采用.采用高速摄影法和影片解析法,对在1997~1998年和1998~1999年全国排球联赛中两次获得最佳发球奖的李铁鸣的跳发球技术进行运动学分析,旨在揭示其技术的运动学特征,探讨影响动作效果的有关因素,为今后的教学和训练提供参考.     

Molecular cloning and expression of interleukin Ibeta (IL-1β) from red seabream (Pagrus major)

The interleukin 1β (IL-1β) cDNA was cloned from the red seabream (Pagrus major) by homology cloning strategy. A cDNA fragment was amplified by PCR using two degenerated primers, which were designed according to the conserved regions of other known IL-1β sequences, and elongated by 3' ends and 5' ends RACE PCR to get the full length coding sequence of red seabream IL-1β (RS IL-1β). The sequence contained 1252 nucleotides that included a 5' untranslated region (UTR) of 84bp, a 3' UTR of 410 bp and an open reading frame (ORF) of 759 nucleotides which could be translated into a putative peptide of 253 amino acids with molecular weight of 28.6 kD and putative isoelectric point pI of 5.29. The deduced peptide contained two potential N-glycosylation sites and an identifiable IL1 family signature, but lacked the signal peptide and the clear ICE cut site, which were common in other nonmammalian IL-1β genes. The RS IL-1β had the highest homology with piscine IL-1β according to phylogenetic tree analysis.     

脑膜瘤的CT、MRI表现与病理对照研究

目的：探讨脑膜瘤的CT、MRI表现与病理分型之间的关系．方法：收集经CT、MRI诊断和手术病理证实的脑膜瘤185例，CT和MRI检查均采用增强前后常规扫描，病理为手术巨检和切片光镜下所见．结果：典型脑膜瘤多为过渡型或纤维母细胞型脑膜瘤，密度(信号)均匀，明显均匀强化，15％～20％伴有钙化，无或轻度瘤周水肿．不典型脑膜瘤以合胞体和血管母细胞瘤型脑膜瘤为主，密度(信号)不均匀，无或不均匀强化，瘤周水肿较重．恶性脑膜瘤为混杂密度(信号)肿块，强化不均匀，形状不规则，瘤周水肿明显，伴有骨质破坏．结论：CT、MRI平扫 增强是诊断脑膜瘤的最主要方法，准确率为95％，在一定程度上可提示脑膜瘤的病理学分型，为术前选择手术方案及判定预后提供信息．     

Development of Full Automatic External Welding Machine for Annular Welds of Pipeline

To meet the demands of rapid development of pipeline constructions in China, a complete set of full automatic external welding machine for annular welds of pipeline and welding procedure have been developed thereof. The system has been applied in the “West-East Pipeline Project” and its performance is proven. With this welding machine the welding parameters can be either preset before or adjusted in real time during the welding process, which avoids the blemishes of same type domestic and international products. Thus it is best propitious to in-situ construction conditions and workers‘ technical level in China. In this article the development of mechanical and control systems of this product is introduced and typical welding procedure parameters are provided.     

制备介孔复合环境材料的酸洗刻蚀工艺

探索了一种制备介孔复合环境材料的方法--破坏式造孔与有机复合相结合,使最终产品可大量吸附污染水体中的各种污染物并具有一定的杀菌功能.该方法通过酸洗刻蚀,达到了去除原材料中的杂质和刻蚀孔径的目的,所制备的中间产品24h吸湿率为原材料的2倍,染料吸附量为原材料的1.6倍.     

极低硫钢的精炼脱硫动力学模型

通过对影响脱硫反应限制性环节的分析,将持续接触和瞬时接触两种反应模式综合考虑,建立了精炼脱硫动力学模型,并通过实验室"极低硫钢精炼脱硫"实验数据对模型进行验证.结果表明,本模型的预测结果与实验结果比较吻合.     

峰谷电价体制下东北输油管网日输油优化研究

东北原油长输管网是中国规模最大的地区性原油运输系统，就该管网基于峰谷电价体制下的运行现状，建立了线性规划数学模型，提出了日输油计划优化问题，并以铁秦线为例进行分析；初步揭示了峰谷电价体制下日输油计划方式的一些基本规律， 表明在该体制下东北管网具有一定的节能降耗潜力。但该方式在一定程度上受到管道本身运行特性的约束，与热油管道相比它更适合于等温管道。