亚硝酰铁氰化纳法测定复杂样品中半胱氨酸含量的方法研究

本文首次建立了亚硝酰铁氰化钠法测定半胱氨酸的方法，该法灵敏度高，选择性好，干扰少，线性范围为１－９０μｇ／ｍＬ，检出极线为０．７８μｇ／ｍＬ，回归方程为ｙ＝０．０１７６ｘ＋０．２１１４，相关系数ｒ＝０．９９９１，尤其适用于复杂样品中半胱氨酸含量的测定。     

川芎嗪对刺激─分泌偶联模型功能活动的抑制作用

用胶原酶消化分离小牛肾上腺髓质嗜铬细胞,１０－４ｍｏｌ／Ｌ乙酰胆碱（Ａｃｈ）促进细胞儿茶酚胺的分泌,其作用具有Ｃａ２＋依赖性,回归方程ｒ＝－３．２９０＋５．２７５ｘ,相关系数Ｒ＝０．９９１０＞＞α０．０１＝０．７９８０．高Ｋ＋（６５ｍｍｏｌ／Ｌ）使膜去极化,也促进细胞儿茶酚胺的分泌,在一定范围内与Ｃａ２＋浓度呈正相关,回归方程ｙ＝１．３７６＋５．３３７ｘ,相关系数Ｒ＝０．９８５６＞＞α０．０１＝０．７９８１．磷酸川芎嗪（ＴＭＰ）浓度为１０－４～１０－７ｍｏｌ／Ｌ时,能抑制Ａｃｈ促进的分泌作用,１０－３～１０－７ｍｏｌ／Ｌ时能抑制高Ｋ＋促进的分泌作用．     

镧存在下一阶导数光谱直接测定饵

在Ｌａ３＋ 、Ｅｒ３＋ 共存的ＲＥ—ＸＯ—ＣＰＣ弱酸性介质体系中,加入Ｆ－ 可有效地掩蔽Ｌａ３＋ 。选用Ｌ１６（４５）正交表进行试验,得到最佳实验条件为：［ ＸＯ］ ＝ １．３１ ×１０－ ４ ｍｏｌ·Ｌ－１ ,［ ＣＰＣ］ ＝ ４ ×１０ －４ ｍｏｌ·Ｌ－１ ,［ Ｆ－］＝ ８×１０４ ｍｏｌ·Ｌ－１ 。一阶导数峰谷法、零谷法、峰零法测定Ｅｒ３＋ 时,３ 倍量的Ｌａ３＋ 不干扰测定,直线回归方程分别为：ｙ＝０ ．２５＋ ０．１２ｘ（ 峰－ 谷法,相关系数０－９９７） ;ｙ＝ ０－１９ ＋０－０８７ｘ（零－ 谷法,相关系数０－９９６） ;ｙ＝ ０－１４ ＋ ０－０２４ｘ（ 峰－ 零法,相关系数０－９８５）。用峰－ 谷法对不同配比Ｌａ３ ＋ 、Ｅｒ３＋ 合成样品进行分析,结果满意。     

桂竹糖芥强心甙G及其制剂HPLC分析

应用高效液相色谱法（ＨＰＬＣ法），以挂竹糖芥甙Ｇ为对照标准品，测定制剂中甙Ｇ的含量．采用μ－ＢｏｎｄａｐａｋＣ１８柱、流动相：乙腈－甲醇－水系统，线性范围：（２．６～７．８）μｇ，变异系数０．９（％），回归方程：ｙ＝１４１５７９２ｘ＋５２６２４．６，相关系数ｒ＝０．９９９９，方法灵敏、准确。     

含两参数的三阶半线性常微分方程边值问题的奇摄动(Ⅰ)

研究含两参数的三阶半线性常微分方程奇摄动边值问题εｙ＋ μｆ（ｘ）ｙ″＋ ｇ（ｘ）ｙ′＝ ｈ（ｘ,ｙ,ε,μ）,ｙ（０） ＝ Ａ（ε,μ） , ｙ′（０） ＝ Ｂ（ε,μ）, ｙ′（１） ＝ Ｃ（ε,μ） ．采用两阶段展开的方法,对（ε／ μ２） →０ （μ→０）的情况构造出形式渐近解,并利用微分不等式理论,证明了解的存在惟一性,同时给出余项的一致有效的估计．     

溶膜富集石墨炉原子吸收光度法测定痕量铬

利用缔合物Ｃｒ（ＨＬ′）２－ＳＣＮ－ＤＢＳ能被可溶滤膜富集的特点,用石墨炉原子吸收分光光度法测定了Ｃｒ（ＶＩ）为０．１μｇ·Ｌ－１级水样。在Ｃｒ（ＶＩ）为１．０～６．０μｇ·Ｌ－１测量范围内,Ｃｒ（ＶＩ）的浓度与吸光度呈良好的线性关系,其相关系数ｒ＝０．９９８８,检测限０．０５μｇ·Ｌ－１。地表水及饮用水中常见离子不影响测定,水样加标回收率为９０％～１１０％。     

幂律流体理论中一类非线性边界层问题

研究了幂律流体理论中一类奇异非线性边界值问题ｇｐ（ｘ）ｇ″（ｘ）＋ｈ（ｘ）＝０,ｋ＜ｘ＜１,ｇ′（ｋ）＝Ｃ,ｇ（１）＝０（ｋ≥０）．ｈ（ｘ）假定为定义在［ｋ,∞）上的连续增函数,满足ｌｉｍｘ→＋∞ｈ（ｘ）ｘσ＞０,Ｃ为任意实数;ｐ,σ均为正常数,ｐ≥１,σ－ｐ＋１≥０．     

Feedback Linearization H_∞ Control and Its Applicationto Excitation Systems

Ｉｎｔｒｏｄｕｃｔｉｏｎ　　Ｃｏｎｓｉｄｅｒｔｈｅｆｏｌｌｏｗｉｎｇｎｏｎｌｉｎｅａｒｕｎｃｅｒｔａｉｎｓｙｓｔｅｍ：·ｘ＝ｆ（ｘ）＋ｇ１（ｘ）ｗ＋ｇ２（ｘ）ｕ,ｚ＝ｈ（ｘ）（１）ｗｈｅｒｅｘ∈Ｒｎ,ｕ∈Ｒｍ,ｗ∈Ｒｐ,ｚ∈Ｒｓａｒｅｓｔａｔｅ,ｃｏｎｔｒｏｌ,ｄｉｓｔｕｒｂａｎｃｅａｎｄｒｅｇｕｌａｔｉｏｎｏｕｔｐｕｔ,ｒｅｓｐｅｃｔｉｖｅｌｙ．ｆ,ｇ１,ｇ２ａｎｄｈ（ｘ）ａｒｅｓｍｏｏｔｈｍａｐｐｉｎｇｗｉｔｈｓｕｉｔａｂｌｅｄｉｍｅｎｓｉｏｎｓ,ａｎｄｆ（０）＝０,ｈ（０）＝０．Ｔｈｅｎｏ…     

多项式自治系统的极限环的唯一性

该文将下列二阶ｎ次多项式自治系统｛ｄｘ／ｄｔ＝１ａ（ｘ）｜ｈ１（ｘ）ｙ，ｄｙ／ｄｔ＝ｇ２（ｘ）＋ｈ２（ｘ）ｙ。其中ｇ１（ｘ）＝Σ（ｎ，ｉ＝０）ａｉｘ＾ｉ，ｈ１（ｘ）＝Σ（ｎ－１，ｉ＝０）ｂｉｘ＾ｉ，ｇ２（ｘ）＝Σ（ｎ，ｉ＝０）ｃｘ＾ｉ，ｈ２（ｘ）＝Σ（ｎ－１，ｉ＝０）ｄｉｘ＾ｉ，变换成Ｌｉｅｎａｒｄ方程、再利用所给引理得到二阶ｎ次多项式自治系统的极限环唯一性的几个充分条件。     

欧拉方程的算子算法

在算子Ｂ＝ｘ．ｄ／ｄｘ作用下,欧拉方程ｘｎｄｎｙ／ｄｘｎ＋Ｐ１ｘ＾ｎ－１ｄｎ－１／ｄｘ＾ｎ－１＋．．．＋Ｐｎ－１ｘｄｙ／ｄｘ＋Ｐｎｙ＝ｆ（ｘ）,其中Ｐ１,Ｐ２,．．．,Ｐｎ为常数）,可化为：（Ａ＾ｎＢ＋Ｐ１Ａ＾ｎ－１Ｂ＋．．．＋Ａ＾０Ｂ）ｙ＝ｆ（ｘ）。并简记为Ｌ（Ｂ）ｙ＝ｆ（ｘ）,把Ｂ待定系数ｋ,则Ｌ（Ｂ）＝０即为欧拉方程的特征方程,从而可求出齐次方程的通解ｙＨ,再根据Ｌ（Ｂ）的逆算子性质求欧拉方程的特解ｙｐ＝１／Ｌ（Ｂ）ｆ（ｘ）,便求得欧拉方程的通解：ｙ＝ｙＨ＋ｙｐ。     

Markedness and its Interpretation in Language Use

Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.     

Features of Women's language

Language is a means of verbal communication. People use language to communicate with each other. In the society, no two speakers are exactly alike in the way of speaking. Some differences are due to age, gender, statue and personality. Above all, gender is one of the obvious reasons. The writer of this paper tries to describe the features of women＇s language from these perspectives： pronunciation, intonation, diction, subjects, grammar and discourse. From the discussion of the features of women＇s language, more attention should be paid to language use in social context. What＇s more, the linguistic phenomena in a speaking community can be understood more thoroughly.     

Characterization of Ordovician carbonate reservoirs, southeastern Saskatchewan, Canada

The discovery of the prolific Ordovician Red River reservoirs in 1995 in southeastern Saskatchewan was the catalyst for extensive exploration activity which resulted in the discovery of more than 15 new Red River pools. The best yields of Red River production to date have been from dolomite reservoirs. Understanding the processes of dolomitization is, therefore, crucial for the prediction of the connectivity, spatial distribution and heterogeneity of dolomite reservoirs.The Red River reservoirs in the Midale area consist of 3～4 thin dolomitized zones, with a total thickness of about 20 m, which occur at the top of the Yeoman Formation. Two types of replacement dolomite were recognized in the Red River reservoir: dolomitized burrow infills and dolomitized host matrix. The spatial distribution of dolomite suggests that burrowing organisms played an important role in facilitating the fluid flow in the backfilled sediments. This resulted in penecontemporaneous dolomitization of burrow infills by normal seawater. The dolomite in the host matrix is interpreted as having occurred at shallow burial by evaporitic seawater during precipitation of Lake Almar anhydrite that immediately overlies the Yeoman Formation. However, the low δ18O values of dolomited burrow infills (-5.9‰～ -7.8‰, PDB) and matrix dolomites (-6.6‰～ -8.1‰, avg. -7.4‰ PDB) compared to the estimated values for the late Ordovician marine dolomite could be attributed to modification and alteration of dolomite at higher temperatures during deeper burial, which could also be responsible for its 87Sr/86Sr ratios (0.7084～0.7088) that are higher than suggested for the late Ordovician seawaters (0.7078～0.7080). The trace amounts of saddle dolomite cement in the Red River carbonates are probably related to "cannibalization" of earlier replacement dolomite during the chemical compaction.     

低渗透非均质砂岩油藏启动压力梯度研究

理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。     

On Tragic Consciousness In The Works By Ernest Hemingway

As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.     

A computer generator for randomly layered structures

AcomputergeneratorforrandomlylayeredstructuresYUJia shun1,2,HEZhen hua2(1.TheInstituteofGeologicalandNuclearSciences,NewZealand;2.StateKeyLaboratoryofOilandGasReservoirGeologyandExploitation,ChengduUniversityofTechnology,China)Abstract:Analgorithmisintrod…     

An Index mechanism for multi-scale view in spatial databases

There are numerous geometric objects stored in the spatial databases. An importance function in a spatial database is that users can browse the geometric objects as a map efficiently. Thus the spatial database should display the geometric objects users concern about swiftly onto the display window. This process includes two operations:retrieve data from database and then draw them onto screen. Accordingly, to improve the efficiency, we should try to reduce time of both retrieving object and displaying them. The former can be achieved with the aid of spatial index such as R-tree, the latter require to simplify the objects. Simplification means that objects are shown with sufficient but not with unnecessary detail which depend on the scale of browse. So the major problem is how to retrieve data at different detail level efficiently. This paper introduces the implementation of a multi-scale index in the spatial database SISP (Spatial Information Shared Platform) which is generalized from R-tree. The difference between the generalization and the R-tree lies on two facets: One is that every node and geometric object in the generalization is assigned with a importance value which denote the importance of them, and every vertex in the objects are assigned with a importance value,too. The importance value can be use to decide which data should be retrieve from disk in a query. The other difference is that geometric objects in the generalization are divided into one or more sub-blocks, and vertexes are total ordered by their importance value. With the help of the generalized R-tree, one can easily retrieve data at different detail levels.Some experiments are performed on real-life data to evaluate the performance of solutions that separately use normal spatial index and multi-scale spatial index. The results show that the solution using multi-scale index in SISP is satisfying.     

Jane Eyre——A Feminist In The 19th Century

In the 19th century the society was controlled by men, and women were just appendants of them, they had not any rights and freedom. But Jane was an exception, she showed some characteristics of early feminist. Jane showed her characteristics of feminism in three aspects: rebellion, equality, and independence. These characteristics were helpful to her success, and feminism is the only way out for women of that time.     

Achieving Unusual States of Matter Under High Pressure

正The periodicity of the elements and the non-reactivity of the inner-shell electrons are two related principles of chemistry,rooted in the atomic shell structure.Within compounds,Group I elements,for example,invariably assume the+1 oxidation state,and their chemical properties differ completely from those of the p-block elements.These general rules govern our understanding of chemical structures and reactions.Using first principles calcula-     

Exchange-Correlation and Electronic Excitation Energies from Pairing Matrix Fluctuations

We have developed an adiabatic connection to formulate the ground-state exchange-correlation energy in terms of pairing matrix linear fluctuations.This formulation of the exchange-correlation energy opens a new channel for density functional approximations based on the many-body perturbation theory.We illustrate the potential of such approaches with an approximation based on the particle-particle Random Phase Approximation(pp-RPA).This re-