Effect of minor Sc on the microstructure and mechanical properties of AZ91 Magnesium Alloy

The as-cast and heat-treated microstructures and mechanical properties of the AZ91 magnesium alloys with and without minor Sc addition were investigated and compared in this paper. The results indicated that adding0.15–0.45 wt% Sc to the as-cast AZ91 alloy not only could modify and refine the Mg_(17)Al_(12) phase but also suppress the formation of the Mg_(17)Al_(12) phase. At the same time, the grains of the Sc-containing as-cast AZ91 alloys were also effectively refined. As a result, the mechanical properties at room temperature(RT) for the Sccontaining as-cast AZ91 alloys were effectively improved. In addition, adding 0.15–0.45 wt%Sc to the AZ91 alloy promoted the formation of the continuous precipitates(CP) during the aging treatment in spite of that the formation of the discontinuous precipitates(DP) was simultaneously suppressed. Accordingly, the Sc-containing as-aged AZ91 alloys obtained the relatively higher mechanical properties at RT than the as-aged AZ91 alloy.     

异步轧制AZ31镁合金板材组织

对不同总变形量、道次压下量、轧制温度以及轧制路径等工艺条件下所制备的AZ31镁合金板材的组织进行研究。研究结果表明：异步轧制有利于板材的晶粒细化,其晶粒粒度约为8．9μm,明显小于常规轧制板材的13．2μm;当总变形量由40％增大到80％时,晶粒粒度从40μm左右减小到30μm左右,出现了较多的孪晶;当道次压下量由5％增加到20％时,晶粒粒度从40μm左右减小到10～20μm,孪晶数量也随之减少;当温度由350℃升高到400℃时,晶粒粒度由20μm左右下降到10μm,且大部分晶粒为等轴晶;轧制路径的改变,使板材中的显微组织和孪晶数量产生改变,C路径中的晶粒细小,粒度约为10μm,D路径中的孪晶数量最少。     

Enhanced mechanical properties of AZ31 magnesium alloy sheets by continuous bending process after V-bending

The effects of V-bending process, continuous bending process and combination process on the microstructure and mechanical properties and formability of an AZ31 magnesium alloy sheet were investigated. The experimental results showed that no twins were found in the microstructure of all samples after processes due to the fine grain. The V-bending and continuous bending processes were proved to be an effective approach to modify the mechanical properties and formability. While the samples after the combination process exhibited better mechanical properties and formability than the single processed sample. The yield strength significantly decreased with the value of 100 MPa and the fracture elongation enhanced to 18.3% at room temperature. The Erichsen value was 5.0 mm which was significantly increased by 117% compared with as-received sample. The superior formability of combination processed samples was mainly attributed to the smaller r-value and n-value.     

碳酸钕对AZ91合金组织的细化和腐蚀性能的影响

通过介绍实验条件实验方法及结果,并对其进行讨论,研究碳酸钕对A291合金组织的细化和腐蚀性能的影响。     

包含式完全正则(T*3(1/2))是相对可乘的

本文讨论包含式完全正则空间（T31/2^＊）关于相对积拓扑的可乘性问题．     

AZ91镁合金热扩渗涂层的研究

采用固体粉末法对AZ91镁合金实施了渗Al、Al-Ce共渗．通过扫描电子显微镜、X射线衍射、能谱和腐蚀测量系统对渗层组织进行了分析．结果表明，该方法能使镁合金表面得到良好的渗层组织，有一定的工程意义．经检验渗Al、Al-Ce渗层均能提高镁合金的耐腐蚀性能，渗Al-ce的耐蚀性更是明显高于渗纯铝．     

抗人Connexin31单克隆抗体的获得与应用

间隙连接蛋白31(Connexin31,Cx31)是间隙连接蛋白(Connexin)家族的一员,目前对于Cx31的功能及其调节方式知之甚少。本实验利用多肽合成的方法合成Cx31羧基端一个多肽片段(250-266AA),经HPLC纯化后偶联到匙孔槭血蓝蛋白,免疫Balb/c小鼠、采血检测产生阳性抗体、脾细胞与骨髓瘤细胞SP2/0融合、筛选阳性克隆建株、分泌的抗体经Westernblotting、细胞免疫荧光染色证实得到的抗体为抗间隙连接蛋白31的特异抗体。     

热处理工艺对触变成形AZ91D镁合金组织的影响

对触变成形AZ91D镁合金在不同热处理条件下的时效组织进行了研究,结果表明:随着固溶温度的增加,第二相具有较大的时效析出速度,并且析出数量较多.经415 ℃、24 h固溶处理后的试样在时效处理过程中,第二相有两种析出方式:连续与不连续析出.在180 ℃没有连续析出,温度高于200 ℃后两种方式交替进行.时效处理温度越高,第二相析出的速度越快.同时也使得连续析出在很短时间内就开始发生,并且在晶粒内部与不连续析出互相交织在一起进行.     

β葡聚糖酶杂合基因bglHAM的克隆及在P.pastoris中的表达

采用PCR的方法,以Bacillus macerans总DNA为模板,构建出β-1,3-1,4葡聚糖酶杂合基因bglHAM,与巴斯德毕赤酵母表达载体pPIC9K重组,得到重组质粒pPIC9K-HAM,电脉冲转化法转化酵母菌GS115,KM71,在MM,MD平板上筛选表型,YPD-G418平板上筛选多拷贝重组子,重组菌株经甲醇诱导后,刚果红平板染色法检测到β-葡聚糖酶活性,SDS-PAGE证明表达产物的分子量约为24kD,摇瓶诱导培养筛选到的重组菌株,胞外每mL发酵液最高酶活达240U。