关于《区间上三段单调扩张自映射的周期轨道》的注记

设m≥0是任一整数.对每一正奇数n≥3,设λn,sn,rn分别是方程xn-2xn-2-1=0,xn-2xn-1-1=0和xn 2-3xn-x2-1=0的唯一正根.记tn0=rn,tni=sn,i≥1,iN,λ=nl→i∞mλn,s=nli→∞msn,t=nli→∞mtn.设λ为f C0(I,I)的扩张常数.利用实分析学中的极限理论,得到了:(1)若f F2(I)∪G2(I),且λ>λ1/2m,则存在最小的奇数n0≥3,使得f有2m.n0-周期点.(2)若f F3(I),且λ>s1/2m,则存在最小的奇数n0≥3,使得f有2m.n0-周期点.(3)若f G3(I),且λ>t1/2m,则存在最小的奇数k0≥3,使得f有2m.k0-周期点.     

N-^-N圈传播子极点漂移小量换序计算

采用核子N（反核子^-N）与中性介子π^2相互作用的Lorentz不变耦合模型，对N-^-N圈图传播子在动量重整化方案中的有限量函数∑c（p）的严格解析计算问题，从极点漂移小量ε作换序计算角度进行了深入的分析、探讨后，发现传播子四维动量平方P^2〉-（核子质量＋介子质量）^2时可作合理换序计算处理．若将此计算结果延拓到P^2≤-（核子质量＋介子质量）^2时，发现与正规计算方法获得的计算结果近似符合程度并非十分理想．     

Synthesis, Characterization and Calorimetry of Ni（C4H8N2O3）2Cl2

A coordination complex was synthesized from NiCl2 and dipeptide glycylglycine（GG）. It was characterized by element analysis, NMR and TG methods, and then was determined to be Ni（C4HsN2O3）2Cl2. Using an isoperibolic reaction calorimeter, the standard molar enthalpy of formation of Ni（GG）2Cl2（solid） has been determined to be -（1 674.66±2.02） kJ · mol^-1 at 298.15 K.     

抚顺煤热解过程中N2生成的实验研究

利用固定床反应器在600~1 300℃范围内进行抚顺煤的热解实验,研究了热解过程中燃料N向N2的转化,以及脱除矿物质元素和添加催化剂对N2生成的影响.升温速率是20℃/min,热解载气为高纯He,热解产生的N2用气相色谱方法定量分析.实验结果表明,抚顺原煤在600℃热解时N2生成量很少,不足10%.随着热解温度的进一步升高,煤中N向N2的转化率几乎呈线性增长.N2的来源一是直接从煤的大分子结构中释放,二是由矿物质元素与燃料氮之间的固相反应产生.抚顺煤脱除矿物质后热解时,N2的生成量明显减少.Ti、Na、K、Fe、Ca类矿物质元素的加入不同程度地促进了N2生成,而且其作用温度区间各不相同.     

N235协同萃取碱性氰化浸金溶液中的金(Ⅰ)

由N235与路易斯碱三辛基氧膦(TOPO)组成协同萃取体系,对碱性氰化浸金贵液中金(Ⅰ)协同萃取和反萃进行了研究.研究了有机相中N235含量、水相平衡pH、相比等因素对金(Ⅰ)萃取率的影响,考察了反萃液中氢氧化钠液浓度对负载金有机相的反萃效果.结果表明,采用有机相为10% 10%协萃剂TOPO 80%煤油的协萃体系,对pH=9～10和初始金(Ⅰ)质量浓度ρo=10.87 mg/L碱性氰化浸金贵液进行萃取时,经一级萃取后,萃取率可高达98%左右;同时,采用0.05～0.1 mol/L的氢氧化钠溶液可对负载有机相进行反萃,反萃率达到91%以上.     

Graft Modification of N,N''''-methylene- bisacrylamide onto Silk in the Presence of Air

The graft modification of N, N'-methylene-bisacrylamide (NNMBAA) onto silk using eerie ammonium sulfate, potassium persulfate, ammonium persulfate and 2, 2-azobis (isobutyronitrile) as the initiators has been studied in the presence of air. To establish reaction conditions for the graft modification of NNMBAA onto silk, the effect of different variables such as the initiator concentration, monomer concentration, acetic acid concentration, time of polymerization, reaction temperature and liquor ratio (fabric: liq.) have been studied. The optimum grafting conditions were found. As evidence of grafting, analyses of amino acid composition and alkali solubility have been carried out. Grafting caused changes in amino acid composition and alkali solubility of silk. The observation has been explained in relation to structural changes in the grafted silk.     

Cloning of aminopeptidase N promoter and its activity in hematopoietic cell and different tumor cell lines

Aminopeptidase N (APN) promoter region was cloned and sequenced from peripheral blood mononuclear cells. The recombinant reporter construct containing the promoter and luciferase gene, designated pXP1-APNLuc, was introduced into myeloblastic cell line, T lymphocyte cell line and various tumor cell lines. Luciferase assay showed that APN upstream promoter is myeloid-specific for high expression in myeloblastic cell line and much lower expression in T lymphocyte cell line. The promoter activity was relatively high in lung adenoma cell line compared with other tumor cell lines including hepatoma cell line, tong cancer cell line and esophageal cancer cell line in which the promoter activity significantly diminished or was almost undetectable. The characteristics of APN promoter may provide a new strategy for specific myeloprotection while tumor patients are being treated with chemotherapy and/or radiotherapy.     

N,N-二甲基甲酰胺二异丙基缩醛对羧酸酯化反应的研究

以N，N－二甲基甲酰胺二异丙基缩醛（简称DMFDIPA）为异丙基化试剂对一些羟酸进行酯化反应。实验表明，DMFDIPA与脂肪酸和芳香酸（高位阻酸除外）都可以发生酯化，酸的强度对反应影响不大。     

胃酸新药莱敏拉唑中间体的合成

以甲苯为原料，通过硝化、还原、酰化、甲基化合成了莱敏拉唑中间体２－甲基－Ｎ－甲基－Ｎ－（２－甲基苯基）－丙酰胺。     

陕西段家坡黄土剖面沉积界线铱的赋存状态及其对N/Q地外撞击事件的启示

采用悬浮沉降法对陕西段家坡黄土剖面第三系—第四系界线样品进行了粒级分选，然后用中子活化分析方法测定了铱和其他微量元素在不同粒级中的含量。实验结果显示，铱在不同粒级物质中的含量按以下顺序增加：粗粉砂（３０～１０５μｍ）＜砂粒（＞１０５μｍ）＜细粉砂（２～３０μｍ）＜粘土（＜２μｍ）。在粘土颗粒物质中，铱的最高含量达８５６ｐｇ／ｇ，较全岩样品富集约１５倍。除了金之外，其他元素（包括Ａｓ、Ｓｂ、Ｂｉ等亲硫元素）在不同粒级中的分布形式与铱显著不同。很显然，铱和其他元素有着不同的来源，界线黄土中铱的异常富集不可能由火山活动或者表生地球化学作用所形成，而极有可能和上新世末（２．４ＭａＢＰ）发生在南太平洋的地外撞击事件有关。这一实验结果表明，南太平洋Ｎ／Ｑ地外物体撞击事件产生的爆炸尘埃可能扩散到了北半球。作为一种近似，以黄土剖面Ｎ／Ｑ界线附近铱的剩余通量作为全球平均，可以估计该撞击物体相当于一直径为２．６ｋｍ的Ｃ１型碳质球粒陨石球体。如此巨大的陨石与地球相撞足以诱发全球性的气候灾变效应