基于超螺旋精度提升机制的OFDM网络信道噪声消除算法

为解决当前OFDM网络信道噪声消除算法难以规避信道中的窄带莱斯噪声,且抗信道衰落能力不强,以及信道间普遍存在严重的频率干涉问题,提出了一种基于超螺旋精度提升机制的OFDM网络信道噪声消除算法.首先,根据各个传输子信道具有差异化的频率载波特性,将传输子信道等价为接收背景中的接收点,从而构建了超螺旋接收结构,有效消除不同传输子信道间存在的频率干扰特性,降低信道窄带莱斯噪声对信号预发射过程的衰落影响;随后,基于角度识别方式进行锐-钝识别,并结合拐点思想,采用序列重排技术,将待发射信号进行消波处理,并进行自旋精度提升,从而提高了其抗窄带莱斯噪声的性能.仿真实验表明:与常见的超高频精度自适应机制(UHF adaptive,UHFA)、共线度自旋精度提升机制(the degree of accuracy of collinear spin,DACS)相比,本文算法与理想状态下的OFDM功率谱密度曲线最为接近,具有更高的信号增益水平与更低的信道误码率.     

The hidden disintegration of cluster heterogeneity in Fe-based glass-forming alloy melt

The evolution of liquid metal at high temperature is known much less than their solid states. This is partially due to that the message concerning clusters, metastable phase or heterogeneity in liquid is usually too slight to be traced. Here, we shed some light on the nature of structural evolution of Fe-based glass-forming alloy during overheating process by the investigation of high-temperature melt viscometry and first principles simulations. It was found that a structural transition around 1400 ℃ occurred in the melts of initial homogeneous ingot, heterogeneous ingot and amorphous ribbons jointly, and was confirmed by the results from differential scanning calorimeter(DSC), and ab initio molecular dynamics(AIMD). Combining these results with Fe-Si-B ternary phase diagram and the melting characteristics of Fe-B compounds, it is safe to conclude that the disintegration of Fe_2B type clusters to Fe_3B-type clusters leads to the observed transition. These results offer a significant reference for the preparation and property control of Fe-based amorphous alloys.     

Template/surfactant free and UV light irradiation assisted fabrication of Mn-Co oxides composite nanorings: Structure and synthesis mechanism

A facile, green, cost effective, and template or surfactant free strategy via a two-step route i.e. UV irradiation followed by dissolution-growth for the controlled synthesis of Mn-Co composite nanorings at room temperature was proposed. The nanorings structures and the process were systematically studied via TEM, HRTEM, EDX and XRD. Bir-MnO_2 nanosheets first formed through the direct photolysis of KMnO_4 under UV light irradiation. This was followed by a dissolution-growth process via the dissolution of Bir-MnO_2 nanosheets by the generated H~+ from the redox reaction between the added Co(NO_3)_2 and residual KMnO_4, as well as the accompanied formation of CoOOH, and Mn-Co composite nanorings. It was found that a balance between the dissolution and growth rate was needed. Suitable pH, KMnO_4 presence and the starting nanosheets like Bir-MnO_2 were the key factors for the formation of nanorings. The obtained Mn-Co nanorings/TiO_2 showed enhanced efficiency for the catalytic oxidation of HCHO. Based on the above understandings, it is believed that the developed dissolution-growth method can be adopted for the designing and preparation of other Mn-Co composite nanostructures which can be further applied for environmental pollution remediation.     

藤黄酸的提取工艺改进

对中药藤黄中的藤黄酸的提取分离进行了方法改进.通过渗漉、吡啶成盐、三次重结晶、置换萃取等步骤得到橙黄色藤黄酸单体.藤黄酸得率为23.9%.并通过IR、MS、1HNMR、13CNMR对藤黄酸进行了结构鉴定.     

结构动力分析中的三维动画显示技术

本文论述了在微机上实现动态图形显示的设计原理及各类变换技术,开发了与结构分析程序SAP80接口的振动模态显示系统ASA2.0（汉化版）。该系统具有分辨率高、占用内存小、运行速度快、动态显示逼真、交互式全汉语菜单提示等一系列特点。     

复杂变质岩矿区构造测量初探

通过对变质岩区地层特征的分析，认为在变质地层中存在着大量的结晶片理、变形分异条带与片麻理条带、构造透镜体、顺层褶皱及近水平韧性剪切带，其分别为纵向构造置换或横向构造置换的结果。为多期变形的产物。在这些地区开展构造测量需考虑采用构造—地层学方法。此工作方法可进一步指导对变质岩老矿山的重新认识与评价。     

渤海湾盆地新生代构造演化

渤海湾新生代盆地经历了早第三纪裂陷沉降和晚期第三纪－第四纪后裂陷热沉降两个阶段。基本完成了一个完整的裂陷作用旋回。早第三纪裂陷作用包括三个裂陷伸展期，它们分别相当于孔店级－沙四段、沙三段、沙二段－沙一段－东营组等三套地层的发育时期，各裂陷伸展期的构造运动学特征有一定的差异，反映在伸展构造样式的变化上，大致可归纳为由多米诺式正断层系统向铲式正断层系统、坡坪式正断层系统的演化序列及由非旋转平面式正断层系统向铲式正断层系统、坡坪式正断层系统的演化序列两个演化模式。     

静水压下加筋圆锥壳振动特性样条分析方法

本文用样条方法分析了静水压下用纵筋和环肋加强的圆锥壳体的振动特性。利用D’Alembert原理建立结构系统的能量变分泛函,由Hamilton变分原理导出运动系统的频率方程。文中导出了样条函数步长矩阵。探讨了水压对加筋圆锥壳振动特性的影响以及不同加筋对振动特性的影响,得到了几点结论。     

辽东湾盆地南部下第三系构造岩相分析

辽东湾盆地由辽西凹陷、辽西低凸起、辽中凹陷、辽东凸起、辽东凹陷五个次级构造单元组成。其下第三系地层包括东上段、东下段、沙一、沙二、沙三与沙四段，发育有九种沉积相、三大沉积体系，根据沉积与构造的配置关系，该区构造岩相带可以划分为五种构造岩相带，如低凸起滨浅湖滩坝型构造岩相带，陡岸半深湖近学水下扇构造岩相带等．构造对沉积的控制规律十分明显，主要表现为不同构造带发育不同的沉积体系，同生断层两侧发育不同的沉积相类型，构造运动的强弱控制沉积体系的发育与分布，不同的构造演化史控制着沉积充填史。受构造岩相双重控制，辽中凹陷的洼中断隆带与坡上断隆带为该区进一步勘探的有利地区。     

吡唑类衍生物的合成与分析

经过酯化、重排和Ｃｌａｉｓｅｎ缩合反应从对甲苯酚和苯乙酸合成了异黄酮的衍生物，再与苯肼反应，得到了嘴唑类衍生物，对反应产物进行了红外，核磁共振，质谱及元素分析测定，并对实验结果进行了讨论。