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1.
以胡萝卜、红枣为原料,利用正交试验设计,主要研究了枣汁浸提的最佳工艺条件以及最佳复合汁配方,并对枣汁的澄清和复合汁稳定进行了探讨.结果表明,最佳浸提条件是:干枣和水质量比为1:7,浸提温度70℃,pH值5.0,浸提时间8h;复合汁最佳配方为:复合汁含量70%,胡萝卜汁/枣汁(V/V)比6:4,糖度14%,柠檬酸量为0.10%;海藻酸钠用量为0.15%时稳定性最好。  相似文献   

2.
本文以新型固体酸SO2-4/Ti-La-O为催化剂,均苯四甲酸二酐和2-乙基己醇为原料,制备均苯四甲酸四(2-乙基己)酯(TOPM)。研究了催化剂的用量、均苯四甲酸二酐和2-乙基己醇的原料配比,反应时间对酯化反应的影响。确定最佳工艺条件:在190℃反应温度下,催化剂用量为3%(以均酐量计);均苯四甲酸二酐:2-乙基己醇为13.5(mol);反应时间为3h。测定TOPM的红外光谱与核磁共振谱,产品收率达97%,酸值<0.1mgNaOH/g,酯含量≥99%。酯化工艺的产品质量高、收率高、工艺简单具有推广应用价值。  相似文献   

3.
本文以新型固体酸SO4^2/Ti-La-O为催化剂,均苯甲酸二酐和2-乙基己醇为原料,制备均苯四甲酸(2-在己)酯(TOPM)。研究了催化剂的用量、均苯四一酐和2-在己醇的原料配比,反应时间对酯化反应的影响。确定最佳工艺条件;在190℃反应温度下,催化剂用量为3%;均苯四甲酸二酐;2-乙基己醇为1:3.5;反应时间为3h。测定TOPM的红外光谱与核磁共振谱,产品收率达97%,酸值〈0.1mgNaO  相似文献   

4.
研究了JA2对刺梨汁的快速澄清作用,测定了经JA2澄清果汁的主要成分变化。结果表明:(1)影响澄清效果的主要因素是果汁的pH值、果汁的浓度和JA2的剂量。(2)经澄清的刺梨汁其透光率可达95%以上;可溶性固形物和总酸含量保持不变;Vc和SOD的损失都小于2%;易使果汁产生二次浑浊和褐变的果胶和单宁类物质的减少率分别为100%和40%。  相似文献   

5.
对叔丁基苯甲酸的合成   总被引:11,自引:0,他引:11  
以对叔丁基甲苯(PTBT)为原料,氧气为氧化剂,冰醋酸为溶剂,醋酸钴为催化剂,考察了合成对叔丁基苯甲苯甲酸(PTBA)的影响因素,确定了该氧化过程的最佳工艺条件:反应温度90~95℃,原料与溶剂配比1:4(m:m),催化剂质量浓度w=0.1~0.2,PTBT的化率可达100%,收率为87%。  相似文献   

6.
利用涤纶废料制取增塑剂DOTP   总被引:4,自引:0,他引:4  
研究了废涤纶料和异辛醇在催化剂作用下,一步合成新型增塑剂--对苯二甲酸二异辛酯(DOTP)的投料配比对产率、产品性能的影响。催化剂及其用量对反应速率的影响,经实验筛选出以钛酸四异丙酯及其复合催化剂,反应温度为210-220℃,原料配比废涤纶:异辛醇=1:(2.8-3.2摩尔比)的最佳工艺条件。  相似文献   

7.
本文研究了超滤法生产柠檬澄清汁的可行性,探讨了膜孔径、温度、压力对澄清汁透液通量和成分的影响。试验结果表明:选用切割分子量为3万的聚丙烯腈膜,在温度50℃、平均压力0.22MPa条件下,能得到稳定的、色泽风味俱佳的澄清汁,其平均透液通量为18.16kg/m2·h。污染的超滤膜用化学清洗液低压湍流清洗,在1小时内,透水通量能恢复到95%以上。  相似文献   

8.
以咖啡因试验A项、B项外观和荧光为指标,采用正交试验法对全合成法制咖啡因(加氢还原)的精制过程中水、高锰酸钾和活性碳的配比;pH值;氧化时间及脱色时间进行了优选。结果表明最佳工艺条件是精制水配比为500%、高锰酸钾配比为1.2%、活性碳配比为5%、pH值为3、氧化时间1.5h、脱色时间1.5h。  相似文献   

9.
对甲苯磺酸催化合成尼泊金乙酯   总被引:5,自引:0,他引:5  
介绍了采用直接酯化法合成尼泊金乙酯的方法,以自制的对甲苯磺酸为催化剂,苯作共沸脱水剂,氧化铝为干燥剂。讨论了反应时间、原料物质的量配比,催化剂用量对收率的影响,确定了最佳工艺条件为n(对羟基苯甲酸):n(乙醇):n(苯):n(对甲苯磺酸)=1:4:1:0.1,反应时间8h,温度78~110℃,酯化反应产率高达86.9%。  相似文献   

10.
对以糯米为原料,采用多菌种共固定化细胞混合技术对发酵生产稠酒进行了研究,实验结果表明,固定化多菌种发酵生产稠酒的最佳发酵工艺如下:多菌种固定化细胞接种配比量为根霉:酿酒酵母:产香酵母:红曲霉=3:1:2:1;固定化凝胶粒子充填量为8%;发酵温度为20℃;发酵时间为96h。  相似文献   

11.
Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.  相似文献   

12.
The Williston Basin is a significant petroleum province, containing oil production zones that include the Middle Cambrian to Lower Ordovician, Upper Ordovician, Middle Devonian, Upper Devonian and Mississippian and within the Jurassic and Cretaceous. The oils of the Williston Basin exhibit a wide range of geochemical characteristics defined as "oil families", although the geochemical signature of the Cambrian Deadwood Formation and Lower Ordovician Winnipeg reservoired oils does not match any "oil family". Despite their close stratigraphic proximity, it is evident that the oils of the Lower Palaeozoic within the Williston Basin are distinct. This suggests the presence of a new "oil family" within the Williston Basin. Diagnostic geochemical signatures occur in the gasoline range chromatograms, within saturate fraction gas chromatograms and biomarker fingerprints. However, some of the established criteria and cross-plots that are currently used to segregate oils into distinct genetic families within the basin do not always meet with success, particularly when applied to the Lower Palaeozoic oils of the Deadwood and Winnipeg Formation.  相似文献   

13.
王慧 《科技信息》2008,(10):240-240
Wuthering Heights, Emily Bronte's only novel, was published in December of 1847 under the pseudonym Ellis Bell. The book did not gain immediate success, but it is now thought one of the finest novels in the English language. Catherine is the key character of this masterpiece, because everybody and everything center on her though she had a short life. We can understand this masterpiece better if we know Catherine well.  相似文献   

14.
The discovery of the prolific Ordovician Red River reservoirs in 1995 in southeastern Saskatchewan was the catalyst for extensive exploration activity which resulted in the discovery of more than 15 new Red River pools. The best yields of Red River production to date have been from dolomite reservoirs. Understanding the processes of dolomitization is, therefore, crucial for the prediction of the connectivity, spatial distribution and heterogeneity of dolomite reservoirs.The Red River reservoirs in the Midale area consist of 3~4 thin dolomitized zones, with a total thickness of about 20 m, which occur at the top of the Yeoman Formation. Two types of replacement dolomite were recognized in the Red River reservoir: dolomitized burrow infills and dolomitized host matrix. The spatial distribution of dolomite suggests that burrowing organisms played an important role in facilitating the fluid flow in the backfilled sediments. This resulted in penecontemporaneous dolomitization of burrow infills by normal seawater. The dolomite in the host matrix is interpreted as having occurred at shallow burial by evaporitic seawater during precipitation of Lake Almar anhydrite that immediately overlies the Yeoman Formation. However, the low δ18O values of dolomited burrow infills (-5.9‰~ -7.8‰, PDB) and matrix dolomites (-6.6‰~ -8.1‰, avg. -7.4‰ PDB) compared to the estimated values for the late Ordovician marine dolomite could be attributed to modification and alteration of dolomite at higher temperatures during deeper burial, which could also be responsible for its 87Sr/86Sr ratios (0.7084~0.7088) that are higher than suggested for the late Ordovician seawaters (0.7078~0.7080). The trace amounts of saddle dolomite cement in the Red River carbonates are probably related to "cannibalization" of earlier replacement dolomite during the chemical compaction.  相似文献   

15.
Location based services is promising due to its novel working style and contents.A software platform is proposed to provide application programs of typical location based services and support new applications developing efficiently. The analysis shows that this scheme is easy implemented, low cost and adapt to all kinds of mobile nework system.  相似文献   

16.
以AC-13级配为基础,将橡胶颗粒代替部分集料掺入混合料中,以低温弯曲试验为评价方法对不同橡胶颗粒掺量下沥青混合料的低温抗裂性进行研究,并引入应变能密度值对混合料的低温抗裂性进行综合评价.试验结果表明:橡胶颗粒沥青混合料试件的破坏微应变均超过2 300,满足冬寒区的技术指标;无论是否掺加橡胶颗粒,随着温度的下降,沥青混合料破坏时的最大弯拉强度增大,弯拉应变降低,劲度模量增大;弯曲应变能密度在胶粒掺量为1%左右时具有较大的弯曲应变能密度值,此时橡胶颗粒沥青混合料具有较好的低温抗裂性.  相似文献   

17.
理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。  相似文献   

18.
Quality traits in wheat (Triticum aestirum L.) were studied by quantitative trait locus (QTL) analysis in a recombinant inbred line (RIL) population, a set of 131 lines derived from Chuan 35050 × Shannong 483 cross (ChSh). Grains from RILs were assayed for 21 quality traits related to protein and starch. A total of 35 putative QTLs for 19 traits with a single QTL explaining 7.99-40.52% of phenotypic variations were detected on 10 chromosomes, 1D, 2A, 2D, 3B, 3D, 5A, 6A, 6B, 6D, and 7B. The additive effects of 30 QTLs were positive, contributed by Chuan 35050, the remaining 5 QTLs were negative with the additive effect contributed by Shannong 483. For protein traits, 15 QTLs were obtained and most of them were located on chromosomes 1 D, 3B and 6D, while 20 QTLs for starch traits were detected and most of them were located on chromosomes 3D, 6B and 7B. Only 7 QTLs for protein and starch traits were co-located in three regions on chromosomes 1D, 2A and 2D. These protein and starch trait QTLs showed a distinct distribution pattern in certain regions and chromosomes. Twenty-two QTLs were clustered in 6 regions of 5 chromosomes. Two QTL clusters for protein traits were located on chromosomes 1D and 3B, respectively, three clusters for starch traits on chromosomes 3D, 6B and 7B, and one cluster including protein and starch traits on chromosome 1D.  相似文献   

19.
As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.  相似文献   

20.
赵英华 《科技信息》2008,(12):219-220
0.Preface China has long been boasting of its colorful and immense culture which comprises of Taoism,Confucianism and Buddhism.The interwoven influence among the religions on Chinese way of thinking,on the nation's behavior in their social life throughout the long history is beyond list.  相似文献   

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