Dielectric relaxation and conduction mechanism in Aurivillius ceramic Bi5Ti3FeO15

For this study, we synthesized Aurivillius Bi5Ti3FeO15 ceramic using the generic solid-state reaction route and then performed room-temperature X-ray diffraction to confirm that the compound had a single phase with no impurities. The surface morphology of the prepared sample was observed to contain microstructural grains approximately 0.2–2 μm in size. The dielectric properties of the sample were determ-ined as a function of frequency in a range of approximately 100 Hz to 1 MHz at various temperatures (303 K ≤ T ≤ 773 K). Nyquist plots of the impedance data were found to exhibit a semi-circular arc in the high-temperature region, which is explained by the equivalent electrical circuit (R1C1)(R2QC2), where R1 and R2 represent the resistances associated with the grains and grain boundaries, respectively, C1 and C2 are the re-spective capacitances, and Q is the constant phase element (CPE), which accounts for non-Debye type of behavior. Our results indicate that both the resistance and capacitance of the grain boundaries are more prominent than those of the grains. The alternating current (ac) conductiv-ity data were analyzed based on the Jonscher universal power law, which indicated that the conduction process is dominated by the hopping mechanism. The calculated activation energies of the relaxation and conduction processes were very similar (0.32 to 0.53 eV), from which we conclude that the same type of charge carriers are involved in both processes.     

基于蓝牙的多功能台灯控制系统设计

针对台灯的个性化和智能化，设计了一套基于蓝牙的多功能台灯控制系统.首先用光敏传感器检测光照强度，用红外感应传感器检测是否有人，用超声波传感器检测使用者与台灯之间的距离，然后将这些检测信号传输到单片机，单片机将信号与设定值进行对比分析，再判断台灯的开/关状态，调节灯光亮度，对使用者的坐姿和使用时间作出语音提醒等.同时，相应参数实时显示在OLED屏和蓝牙终端，使用者通过蓝牙终端可以对台灯进行控制.与蓝牙的联机测试结果显示，系统功能强大，运行稳定.     

Effect of Co substitution on the structural,dielectric and optical properties of KBiFe2O5

Cobalt (Co)-modified brownmillerite KBiFe2O5 (KBFO; [KBiFe2(1?x)Co2xO5 (x = 0, 0.05)]) polycrystalline is synthesized following the solid-state reaction route. Rietveld refinement of X-ray diffraction data confirmed the phase purity of KBFO and KBiFe1.9Co0.1O5 (KBFCO). The optical bandgap energy (Eg) of KBFO decreased from 1.59 to 1.51 eV because of Co substitution. The decrease in bandgap can be attributed to the tilting of the Fe–O tetrahedral structure of KBFCO. The observed room-temperature Raman peaks of KBFCO shifted by 3 cm?1 toward a lower wavenumber than that of KBFO. The shift in Raman active modes can be attributed to the change in the bond angles and bond lengths of the Fe–O tetrahedral structure and modification in response to oxygen deficiency in KBFO because of Co doping. Compared with that of KBFO, the frequency-dependent dielectric constant and dielectric loss of KBFCO decrease at room temperature, which is a con-sequence of the reduction in oxygen migration and modification in response to vibrational modes present in the sample.     

Corrosion behavior of cold-rolled and post heat-treated 316L stainless steel in 0.9wt%NaCl solution

The effect of cold rolling and post-rolling heat treatment on the microstructural and electrochemical properties of the 316L stainless steel was investigated.Two-pass and four-pass cold-rolled stainless steel specimens were heat-treated by annealing at 900℃followed by quenching in water.During the cold rolling,the microstructure of the as-received specimen transformed from austenite to strain-inducedα′-martensite due to significant plastic deformation that also resulted in significant grain elongation(i.e.,~33%and 223%increases in the grain elongation after two and four rolling passes,respectively).The hardness of the heat-treated as-received specimen decreased from HV 190 to 146 due to the recovery and recrystallization of the austenite grain structure.The cyclic polarization scans of the as-rolled and heat-treated specimens were obtained in 0.9wt%NaCl solution.The pitting potential of the four-pass rolled specimen was significantly increased from 322.3 to 930.5 mV after post-rolling heat treatment.The beneficial effect of the heat treatment process was evident from~10-times-lower corrosion current density and two-orders-of-magnitude-lower passive current density of the heat-treated specimens compared with those of the as-rolled specimens.Similarly,appreciably lower corrosion rate(3.302×10^?4mm/a)and higher pitting resistance(1115.5 mV)were exhibited by the postrolled heat-treated specimens compared with the as-rolled 316L stainless steel specimens.     

Al涂层/AZ91镁合金复合铸造界面的研究

对型芯预喷涂一层Al涂层,将AZ91镁合金液浇注到铸型中实现基体和涂层的结合,对凝固后的结合界面组织和相组成进行分析。结果表明,AZ91镁合金液和Al涂层表面的氧化物发生反应,实现了界面间的润湿,形成冶金结合界面。该界面包含3个扩散层:镁合金基体一侧为(Al₁₂Mg₁₇+δ_Mg)共晶组织;中间层为Al₁₂Mg₁₇金属间化合物;Al涂层一侧为Al₃Mg₂金属间化合物,并弥散分布着一些氧化物。试验结果证明,通过复合铸造的方法可以实现Al涂层和镁合金基体的冶金结合。     

拉瓦尔喷管中的气流状态参数计算分析

本文使用微分形式与差分形式的气流状态方程推导并结合MATLAB软件编程计算分析了超音速进口以及超音速出口情况下的拉瓦尔喷管内沿轴向分布的各位置处的气流参数压强、温度、密度、速度的分布特点。分析计算与仿真结果发现,气流马赫数M在喷管喉道达到了最小值,而温度T、压强P、密度ρ等参数则在喉道处达到了峰值;喉道处马赫数随着初始进口马赫数的提高而增大;计算结果的残差分析表明随着科朗数C的增大,计算收敛所需步数减少,但残差峰值也随之增大,当科朗数C=1.75时计算结果发散。     

开关磁阻电机调速系统技术分析与应用展望

开关磁阻电机调速系统是将控制技术、现代电力电子技术和开关型磁阻电机融合于一体的综合性系统,具有构成简洁、坚固、耐用、可靠等优点。基于此,本文首先介绍了开关磁阻电机调速系统的主要特点,然后对开关磁阻电机调速系统在不同领域的应用进行了分析与展望,阐明了该技术在各行业中的应用价值。     

潮白河下游晚更新世晚期-全新世早期地层粒度特征

通过潮白河下游第四纪剖面测量,采集光释光样品2个,显示剖面年龄为(12.36±1.76)~(5.15±0.80)ka,沉积时代为晚更新世晚期到全新世早期。结合地层厚度,计算出该地区平均沉积速率为0.038 cm/a。采集并测试37个粒度样品,频率曲线特征是双峰、左偏双峰、右偏双峰及三峰,说明沉积物成分复杂。概率累计曲线特征是三段式,滚动组分含量存在变化,说明水动力条件存在强弱的更替。地层自下而上沉积模式是黏土-粉砂-粉砂质黏土。结合区域地质特征,综合分析潮白河下游晚更新世晚期-全新世早期沉积环境为泛滥平原沉积。本文研究结果可为潮白河下游沉积过程研究、地下水综合利用与开发提供重要地质资料。