微波合成PMMA胶乳粒子

在常压微波辐照下合成聚甲基丙烯酸甲酯（ＰＭＭＡ）单分散的胶体微粒。体系中未加表面活性剂和稳定剂,在透射电镜下观察粒子的形状和直径大小,并得出在引发剂浓度一定的条件下,微粒的体积与单体的浓度呈现线性关系,为我们合成一定大小的超细微粒提供了选择的条件。功力学实验表明,微波场下反应速度大大加快,反应是突变的,无恒速阶段。     

激光热致相变核-壳微胶囊的合成与性能

以甲基丙烯酸甲酯作为主要的核单体，甲基丙烯酸缩水甘油酯作为壳单体，叔胺盐作为壳的改性剂，合成了平均粒径为55nm具有激光热致相变性能的核壳微胶囊。用红外光谱对其结构进行了表征；用透射电镜观察了微胶囊形貌；用示差量热分析法、热重分析法测定了热性能、接触角仪测定了相变前后的亲水性，探讨了对相变效果的影响因素。核聚合物的玻璃化转变温度为56.2℃，壳聚合物的玻璃化转变温度为85.3℃；该微胶囊感激光后发生相变，接触角由初始的20°变为93°。     

Influences of Electrolytes on Soap-Free P(ST-MMA-AA) Emulsion Polymerization

1Introduction Functional polymer microspheres are kinds of polymer particles with special structures, morphologies or functional groups[1] , and have been gained much attention because of their specific properties and their application since 1980s. Although some researches have investigated that the latex particle size and its distribution,as well as the stability of polymerization and the resultant latex were strongly influenced by introducing electrolyte into the emulsion polymerization system[2] , few of them focused on the systematic study of electrolytes on the soap-free emulsion polymerization, which is considered as a conventional approach to synthesize functional polymer microspheres with clean surfaces[2]. In this presentation, the influences of variety and dosage of electrolytes on soap-free emulsion polymerization of St, MMA and AA were studied, and a series of micron or submicron sized latex particles with narrow distribution were obtained.     

数字合成波形发生器设计

以单片机为核心，对数字波形表各项进行比例换算和线性叠加的数字合成处理。采用定时器中断方式将处理结果经D／A口输出；并对输出信号进行放大、单到双极性变换和滤波处理，获得数字合成的波形信号．通过按键编辑任意波表，改变定时器参数和比例因子，达到任意波获取、波形频率和幅度数字调节目的．采用8住LED显示器动态刷新方式。显示波形类型、频率和幅度．     

环氧树脂基纳米复合材料的研究进展

介绍了环氧树脂基纳米复合材料的性能、制备方法、作用机理及其研究进展。     

纳米尺寸聚合物胶乳及其粒径分布

用半连续乳液聚合法合成了粒径为５０ｕｍ～１００ｕｍ的苯乙烯－丙烯酸了酯－丙烯酸共聚物胶乳，讨论了搅拌速度等其它因素对胶乳粒度及分布的影响．实验表明，增加乳化剂量有利于胶乳粒度减小，但超过一个阔值将使粒径分布变宽．     

烧结矿配料优化计算模型的设计

炼铁厂进行烧结矿配料时,当铁矿粉种类较少时,配料计算非常简单,当铁矿粉超过5种以上时,就难以通过普通多项式进行计算。建立一种多矿种铁矿粉最优化配矿组合数学模型并编写了相关程序,可输出满足烧结矿成份要求、相对该种配矿组合价格最低的铁矿粉配矿组合。     

Influences of Electrolytes on Soap-Free P（ST-MMA-AA） Emulsion Polymerization

1 Introduction Functional polymer microspheres are kinds of polymer particles with special structures, morphologies or functional groups~([1]), and have been gained much attention because of their specific properties and their application since 1980s. Although some researches have investigated that the latex particle size and its distribution, as well as the stability of polymerization and the resultant latex were strongly influenced by introducing electrolyte into the emulsion polymerization …     

浅谈增稠剂种类及其在乳胶漆生产中的作用

主要从增稠机理的角度,分析了增稠剂种类、用量对乳胶漆施工性能及贮存稳定性的影响。     

试论义位的组合关系

义位之间的组合关系是相当复杂的,它的深入分析将对句义的组合以及词语的各种结构关系的研究提供一些便利条件。我们从语言现实出发,根据义位在语流交际中的搭配情况,归纳出了17种主要的组合关系。