氯代羟基二苯醚合成工艺的改进

对以取代酚和硝基氯苯为原料，采用缩合、还原、重氮化、水解制备氯代羟基二苯醚的合成工艺进行了改进。提出了一种无溶剂熔融醚缩合方法，并优化了氨基二苯醚重氮盐水解的条件，使其合成方法具有更好的工业应用前景。     

自由曲线与正弦曲线合成曲线的研究

本文提出自由曲线和正弦曲线合成的方法,通过调整正弦曲线的幅值和频率,改变合成曲线的形状,这种方法易于实现和分解,并可用于描述随机形状.     

气体输运过程的讨论

采用简化假设的理论和考虑到气体分子自由程的分布及麦克斯韦速度分布律的初级理论这两种方法近似计算输运系数，并指出简化假设理论与实际情形的差异，同时就简化假设理论能得到与精确程度较高的初级理论相同结果的原因进行讨论。     

BA模型的三种扩展

无标度网络的发现，使人类对于复杂网络的认识进入了一个新的天地．BA模型是对于这种新认识的第1个抽象模型．由于考虑了系统的成长性和连接的择优性，BA模型给人们带来了很多启发．但是BA模型的两个基本假定，对于解释许多现实中的现象来说过于简单，与现实的网络还有较大的距离．所以，作者试图对BA模型进行扩展，即根据现实中的网络，增添某些假定，并通过计算机模拟进行观察，以便进一步探索复杂网络系统的规律．对BA模型的扩充考虑了3个因素：择优选择的成本；边的重新连接；网络的初始状态．实验结果表明，在考虑了这些因素之后，BA模型的基本结论并没有变化，它们的影响在于演化过程的某些方面，例如在某些极端条件下的演变趋势等．     

Geochemical study and significance of sequential extraction in reservoir rocks of Turpan-Hamin Basin

Seven samples collected from the Turpan-Hamin Basin were treated by sequential extraction method. Analytical results indicate that the free oils, inclusion oils (oil-bearing fluid inclusions) and clay-adsorbed oils vary significantly. The geochemical characteristics of inclusion and clay-adsorbed oils correlate well with the lacustrine mudstones. The characteristics are as follows: (i) with higher Ph/nC18 ratio and lower Pr/Ph ratio; (ii) with higher values of C26 tricyclic/C24 tetracyclic terpane, C23 tricyclic ter-pane/(C23 tricyclic terpane+C3017α(H) hopane), C21/(C21+C29) sterane, Ts/Tm and C29Ts/C29l7α(H) norhopane and lower value of C19/C21 tricyclic terpane; (iii) with relatively high content of C27 and C28 sterane and lower abundance of C29 sterane and diasterane. They indicate that the early charged oils are derived from the pre-Jurassic lacustrine mudstones and the later charged oils are from the Jurassic coal-bearing strata or coals.     

碳纳米管对聚苯乙烯分子运动的影响

利用DSC、流变仪和能量损耗仪等测试仪器,系统研究了碳纳米管加入到聚苯乙烯基体中后对不同长度聚苯乙烯分子链运动的影响.结果表明,碳纳米管加入到聚苯乙烯中后对聚苯乙烯的玻璃转变和液-液转变都产生了影响.碳纳米管的加入引起自由体积的增加只在一个很小的范围内影响了分子链段的运动,当质量分数为0.1%的碳纳米管加入时,链段运动速度增加,玻璃转变温度明显向低温方向移动;而由于范德华力的存在,高分子链会在碳纳米管表面选择吸附,从而使得整链运动时,参与运动的链单元尺寸降低,所以造成了整链运动时链间的耦合降低了.     

Template/surfactant free and UV light irradiation assisted fabrication of Mn-Co oxides composite nanorings: Structure and synthesis mechanism

A facile, green, cost effective, and template or surfactant free strategy via a two-step route i.e. UV irradiation followed by dissolution-growth for the controlled synthesis of Mn-Co composite nanorings at room temperature was proposed. The nanorings structures and the process were systematically studied via TEM, HRTEM, EDX and XRD. Bir-MnO_2 nanosheets first formed through the direct photolysis of KMnO_4 under UV light irradiation. This was followed by a dissolution-growth process via the dissolution of Bir-MnO_2 nanosheets by the generated H~+ from the redox reaction between the added Co(NO_3)_2 and residual KMnO_4, as well as the accompanied formation of CoOOH, and Mn-Co composite nanorings. It was found that a balance between the dissolution and growth rate was needed. Suitable pH, KMnO_4 presence and the starting nanosheets like Bir-MnO_2 were the key factors for the formation of nanorings. The obtained Mn-Co nanorings/TiO_2 showed enhanced efficiency for the catalytic oxidation of HCHO. Based on the above understandings, it is believed that the developed dissolution-growth method can be adopted for the designing and preparation of other Mn-Co composite nanostructures which can be further applied for environmental pollution remediation.     

G-调和函数增长性及其在二相自由边界问题上的应用

研究了G-调和函数的增长性,给出其在二相空腔与射流问题上关于极小化子增长性的应用.     

本土化视域下影视字幕翻译策略研究

字幕翻译应通过对源语信息进行浓缩、简化、省略等减译处理,给观众提供通俗易懂、简洁流畅且符合人物个性的字幕语言,让观众迅速准确地明白剧情。翻译的难度在于文化信息的转换,翻译时应尽力保留源语独特的表达方法,诸如词语、比喻、典故、人名等应直译,以体现源语及其文化的瑰丽;不得已时,再采用意译,以达到与源语功能的对等。意译时,可采用适度的娱乐化改写或本土化策略。     

公共图书馆“免费开放”相关问题探究

在对公共图书馆收费项目性质进行系统分析的基础上,论述了"免费开放"的范围与程度,对免费开放后如何在保证公益性的前提下弥补经费不足的问题进行了探讨,强调了免费开放后应对国家、地方财政的资金投入制定切实可行的绩效评价机制。