胶体金标记牛血清白蛋白及其在电场中的迁移行为

采用柠檬酸钠还原法制备了不同粒径的胶体金,对牛血清白蛋白(BSA)进行标记,考察了胶体金标记BSA的影响因素.以琼脂糖凝胶为载体介质,研究了三种粒径的胶体金及其BSA复合物在电场中的迁移行为.结果表明,pH值、离子浓度、蛋白量都会影响胶体金对BSA的标记.标记的最适条件是:无盐或极低盐浓度,pH值5.8,蛋白加入量不小于最小稳定蛋白量.胶体金及其BSA复合物在特定电场中的迁移行为类似于火箭免疫电泳,其迁移速度随着金纳米粒子粒径的增大而减小;金纳米粒子与BSA结合后迁移速度减慢,BSA的加入量对复合物的迁移速度无影响.     

Preparation of modified SiO2 colloidal spheres with succinic acid and the assembly of colloidal crystals

SiO2 colloidal spheres were synthesized by St-ber method. In order to enhance surface charge of the SiO2 spheres, they were modified with succinic acid. Scanning electron microscope (SEM) shows that the average size of modified SiO2 spheres is 473 nm, and its distribution standard deviation is less than 5%; Fourier-transform infrared spectra (FT-IR) and X-ray photoelectron spectrometer (XPS) results indicate that one end of succinic acid is chemically bonded to the SiO2 spheres through esterification; Zeta potential of the modified SiO2 spheres in water solution is improved from -53.72 to -67.46 mV, and surface charge density of the modified SiO2 spheres is enhanced from 0.19 to 0.94 μC/cm2. SiO2 colloidal crystal was fabricated from aqueous colloidal solution by the vertical deposition method at 40℃ and 60% relative humidity. SEM images show that the sample of SiO2 colloidal crystal is face-centered cubic (fcc) structure with its (111) planes parallel to the substrate. Transmission measurement shows the existence of photonic band gap at 1047 nm.     

The research and progress of micro-fabrication technologies of two-dimensional photonic crystal

The novel material of photonic crystal makes it possible to control a photon, and the photonic integration will have breakthrough progress due to the application of photonic crystal. It is based on the photonic crystal device that the photonic crystal integration could be realized. Therefore, we should first investigate photonic crystal devices based on the active and the passive semiconductor materials, which may have great potential application in photonic integration. The most practical and important method to fabricate two-dimensional photonic crystal is the micro-manufacture method. In this paper, we summarize and evaluate the fabrication methods of two-dimensional photonic crystal in near-infrared region, including electron beam lithography, selection of mask, dry etching, and some works of ours. This will be beneficial to the study of the photonic crystal in China.     

合肥光源深X-射线光刻模拟

论文对合肥同步辐射光源开展深度X-射线光刻进行了理论模拟。利用Gauss积分法研究了菲涅耳衍射对深度光刻图形精度的影响。为了模拟衬底产生的光电子对光刻结果的影响，构建了一个Monte Carlo模型并进行了模拟。计算结果表明，合肥光源深度光刻的图形精度较高。     

垂直沉积法制备二氧化硅胶体晶体及其表征

利用垂直沉积法将单分散的二氧化硅胶体微球自组装生长为胶体晶体 ,并用扫描电子显微镜和紫外可见光分光光度计对其显微形貌和光学特性进行了表征 .结果表明二氧化硅微球有序堆积 ,自组装成胶体晶体 ,其结构为FCC密排结构 ,表面为FCC密排结构的 ( 1 1 1 )面 ;反射光谱还表明 ,所制备的胶体晶体的光子带隙位于可见光波段 .与重力沉淀等其他自组装方法相比 ,垂直沉积法制备胶体晶体具有能够用胶体微球粒径和胶体溶液浓度精确控制样品厚度等优点     

用亚纳米技术生产特种水泥

将亚纳米技术应用于水泥熟料煅烧、粉磨等工序中，以提高熟料标号、粉体细度、比表面积等，生产出道路耐磨、快硬、早强水泥及硫铝（铁）酸盐等特种水泥．     

Nano-and Micro-patterned Biomaterials

1 Results Our objective is two fold: we (ⅰ) aim at the development of novel patterning methodologies in order to (ⅱ) achieve control over the positioning and alignment of living cells.The patterning of the biointerfaces is carried out both at the micro-and nanometer scale and involve (bio)chemical as well as topographic patterns.The former are relatively easily obtained by patterning techniques adapted from (conventional) soft lithography,e.g.by means of micro-contact printing (μ-CP).The topographic pat...     

亚波长光刻离轴照明和次分辨率辅助图形技术

讨论了亚波长光刻条件下的离轴照明和次分辨率辅助图形两种分辨率的增强技术,分析了两种技术的原理,利用光刻模拟软件,针对不同线宽的稀疏线条,对添加次分辨率辅助图形前后的光刻仿真结果进行了对比.研究结果表明,离轴照明技术和次分辨率辅助图形的结合使用,可以显著提高亚100纳米级版图线条的光刻分辨率,增大工艺窗口,降低版图成像对生产工艺参数的要求,对于解决亚波长光刻所带来的亚100纳米级集成电路成像质量下降的问题非常必要.     

功能性纳米溶胶CdS的合成与荧光性质研究

报道了无机纳米溶胶CdS的合成,并对其进行了功能化修饰,同时研究了功能CdS纳米溶胶的荧光性质。     

钛酸钠纳米线的电传输特性研究

利用电子束光刻技术制作了基于钛酸钠纳米线的纳米器件。分别在大气和真空两种环境下测量了该器件的电学特性,发现器件所处的气体环境可以影响其电传输特性,这可能是由于纳米线表面的氧分子吸附造成的。另外,还研究了紫外光（UV）照射纳米线对器件电学特性的影响,发现紫外光可以使纳米线产生很大的光电导。研究表明上述纳米器件可用作气体探测器和光电探测器。