正交试验法优选坚龙胆中龙胆苦苷的提取工艺

目的:优选坚龙胆中龙胆苦苷的提取工艺.方法:以龙胆苦苷的含量为指标,采用高效液相色谱法进行含量测定,采用L9(34)正交设计试验,对提取次数、提取溶剂倍数和提取时间3因素进行考察,以确定最佳提取工艺.结果:提取3次,用10倍量的甲醇,提取时间每次20min为最佳提取工艺.结论:该工艺合理,且稳定可行.     

炉膛喉口面积对W型火焰锅炉炉内空气动力场的影响

对珞璜电厂引进法国Ｓｔｅｉｎ公司３６０ＭＷ的Ｗ型火焰锅炉进行了冷态模化研究。采用热线风速仪对炉内流场进行测试,在此基础上研究了炉膛喉口面积对炉内空气动力场的影响规律,得出了在不同相对喉口面积下的炉内气流流场图,并对炉内的气流速度分布,气流充满度和平均有效动量流率等进行了比较与分析。研究表明,适当缩小炉膛喉面积,王方面有利于喷入炉内煤粉的着火和燃尽,另一方面有利于减小高温烟气对喉口和前,后拱及冷灰斗     

鬼臼乙叉甙诱导NB4细胞凋亡的实验研究

为了从细胞凋亡角度探讨鬼臼乙叉甙（4′－demethylepipodophyllotoxin-9-4(4,6-O-ethylidene-β－D－glucopyranoside）抗肿瘤作用的机理。用活细胞计数法,克隆形成法及MTT比色法观察了其对NB4细胞的生长抑制作用;用光学显微镜及电子显微镜观察了凋亡细胞的形态学变化;用琼脂糖凝胶电泳观察了DNA的梯形改变。结果发现：鬼臼乙叉甙能显著抑制NB4细胞的生长增殖及诱导其凋亡,诱导凋亡是鬼臼乙叉甙抗肿瘤作用的机理之一。     

适应于机器人机构的运动学递推公式

本文对工业机器人机构进行运动学分析，建立通用的运动学递推公式；将奇异值分解（ＳＶＤ）理论应用到运动学逆问题数值解中，避免机器人机构的奇异状态。     

论启发式例题的编选

讨论如何编选启发式例题，才能激发学生学习数学的积极性，提高数学教学效果，论述均以最新资料为依据。     

一类微分算子的亚椭圆性与局部可解性

考虑形如P=(D_t—iat~kD_x~l)(D_l—ibt~kD_x~l)+ct~(k-1)D_x~l的一类线性微分算子,给出其在原点亚椭圆性与局部可解性的条件。     

Synthesis and structure determination of ruthenium and osmium complexes with 2,6-bis-(diphenylphosphinomethyl) pyridine

2,6-Bis (diphenylphosphinomethyl) pyridine (PNP) reaction with Na₂OsCl₆ · 6H₂O to give the five coordinated, sixteen-electron complex Os (PNP)Cl₂. In the presence of formaldehyde, the reaction between Na₂OsCl₆· 6H₂O and PNP proceeds rapidly in boiling ethanol to give the coordinately saturated Os(PNP)Cl₂(CO). The IR spectrum of Os(PNP)Cl₂(CO) shows a strong absorption band at 1 970 cm⁻¹ assignable tov _∞ stretch. PNP reacts with RuCl₂(PPh₃)₃ and RuCl₂(DMSO)₄ (DMSO=dimethyl sulfoxide) to give Ru(PNP)Cl₂ (PPh₃) and Ru(PNP)Cl₂ (DMSO) respectively. The average Ru−Cl, Ru−P and Ru−N bond distance in Ru(PNP)Cl₂(PPh₃) determineby X-ray crystallography are 0.242, 0.236 and 0.216 nm, respectively. Li Zhaoying: born in July 1949, associate professor     

《管子》“以法治国”的法制思想探析

早在春秋时期,管子就已提出了"以法治国"的思想。他提出,法应当成为天下人共同遵循的礼,主张把法看成是评判是非的标准;法不是一种高高在上的空洞的法律条文,且法的有效施行要求执行法律的统治者公正无私、信赏必罚;法为治平之术,法能兴功立事。虽然管子的思想受到当时时代条件的局限,但深入挖掘其法制思想内涵,对于我们现今"以法治国"有着非常重要的启示。     

解读大学生中的武侠热现象

武侠小说在大学生中流传甚广.文章从文化的视角对大学生喜读武侠小说这一现象进行深入地剖析,由浅入深,由表及里,探寻这一现象背后深刻的文化根源.     

Genome-wide association study identifies five loci associated with susceptibility to pancreatic cancer in Chinese populations

Pancreatic cancer has the lowest survival rate among human cancers, and there are no effective markers for its screening and early diagnosis. To identify genetic susceptibility markers for this cancer, we carried out a genome-wide association study on 981 individuals with pancreatic cancer (cases) and 1,991 cancer-free controls of Chinese descent using 666,141 autosomal SNPs. Promising associations were replicated in an additional 2,603 pancreatic cancer cases and 2,877 controls recruited from 25 hospitals in 16 provinces or cities in China. We identified five new susceptibility loci at chromosomes 21q21.3, 5p13.1, 21q22.3, 22q13.32 and 10q26.11 (P = 2.24 × 10(-13) to P = 4.18 × 10(-10)) in addition to 13q22.1 previously reported in populations of European ancestry. These results advance our understanding of the development of pancreatic cancer and highlight potential targets for the prevention or treatment of this cancer.