| 2-苯基噻唑烷-4-甲酸的微波合成研究 |
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| 引用本文： | 杜娟,高文秀.2-苯基噻唑烷-4-甲酸的微波合成研究[J].松辽学刊,2007,28(4):92-93. |
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| 作者姓名： | 杜娟 高文秀 |
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| 作者单位： | 吉林师范大学化学学院,吉林四平136000 |
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| 摘 要： | 在微波常压反应条件下，用L-半胱氨酸合成了2-苯基噻唑烷—4-甲酸，讨论了反应时间、微波功率以及反应物用量对产率的影响．实验表明，微波技术可用于光学活性化合物的合成，并显示出微波合成的简便、安全、快速、产率高的特点．
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| 关 键 词： | 微波 辐射 缩合 2-苯基-噻唑烷-4-甲酸 |
| 文章编号： | 1000-1840-（2007）04-0092-02 |
| 收稿时间： | 2007-10-08 |
| 修稿时间： | 2007年10月8日 |
Study on Rapid Synthesis of 2-Phenyl-Thiazolidine-4-Carboxylic Acid under the Irradiation of Microwave |
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| DU Juan,GAO Wen-xiu.Study on Rapid Synthesis of 2-Phenyl-Thiazolidine-4-Carboxylic Acid under the Irradiation of Microwave[J].Songliao Journal (Natural Science Edition),2007,28(4):92-93. |
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| Authors: | DU Juan GAO Wen-xiu |
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| Institution: | DU Juan, GAO Wen - xiu (College of Chemistry,Jilin Normal University,Siping 136000, China) |
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| Abstract: | 2-phenyhhiazolidine-4-earboxylic acid was prepared from L-cysteine under the irradiation of microwave conventional pressure. The feasibility of microwave technology in synthesizing optical active compounds was examined and the influence of microwave power and reaction time on the yield was discussed as well. The results show that microwave technology is a method of simplity,secufity,rapidity with a high yield. |
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| Keywords: | microwave radiation condensation 2-phenyl-thiazolidine-4-carboxylic acid |
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