| PEG-400-水体系中四组分一锅法合成多氢喹啉衍生物 |
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| 引用本文： | 王进贤,孙永军.PEG-400-水体系中四组分一锅法合成多氢喹啉衍生物[J].西北师范大学学报,2011,47(2). |
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| 作者姓名： | 王进贤 孙永军 |
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| 作者单位： | 西北师范大学化学化工学院; |
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| 基金项目： | 国家自然科学基金资助项目(20272047,20572086); 甘肃省自然科学基金资助项目(3ZS051-A25-001) |
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| 摘 要： | 以1,3-环己二酮、取代醛、乙酰乙酸乙酯、醋酸铵为原料,在PEG-400-水体系中合成了一系列多氢喹啉类化合物.除对所有化合物进行红外光谱和核磁共振谱表征外,对未报道的化合物也进行了质谱和元素分析结构确证.结果表明,该方法具有反应时间短、操作简单、产率高等优点,符合绿色化学的要求.
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| 关 键 词： | 多氢喹啉 合成 PEG-400 |
Four-component one-pot synthesis of polyhydroquinolines in PEG-400-water system |
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| WANG Jin-xian,SUN Yong-jun.Four-component one-pot synthesis of polyhydroquinolines in PEG-400-water system[J].Journal of Northwest Normal University Natural Science (Bimonthly),2011,47(2). |
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| Authors: | WANG Jin-xian SUN Yong-jun |
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| Institution: | WANG Jin-xian,SUN Yong-jun (College of Chemistry and Chemical Engineering,Northwest Normal University,Lanzhou 730070,Gansu,China) |
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| Abstract: | An efficient one-pot synthesis of polyhydroquinolines is achieved using aldehydes,1,3-cyolohexanedione,ethyl acetoacetate,and ammonium acetate,in which a four-component reaction is operated in PEG-400-water system.A series of polyhydroquinolines compounds are characterized by IR and NMR spectroscopy.The reaction has the following advantages:easy manipulation,short reaction time,environmentally-benign and high yield. |
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| Keywords: | polyhydroquinolines synthesis PEG-400 |
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