| 1—[5—（4—硝基苄基）—2H—四唑乙酰基]—4—芳酰氨基硫脲的合成 |
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| 引用本文： | 孙乐,王哨兵.1—[5—（4—硝基苄基）—2H—四唑乙酰基]—4—芳酰氨基硫脲的合成[J].兰州大学学报(自然科学版),1998,34(3):77-81. |
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| 作者姓名： | 孙乐 王哨兵 |
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| 作者单位： | 兰州大学化学系应用有机国家重点实验室 |
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| 摘 要： | 利用５－（４－硝基苄基）－２Ｈ－四唑－２－乙酰肼与芳基异硫氰酸酯在无水丙酮中反应，制得１０种新的－１－〔５－（－４－硝基苄基）－２Ｈ－四唑乙酰基〕－４－芳酰氨基硫脲。所有化合物结构经元素分析、红外、＾１Ｈ ＨＭＲ和质谱方法确认，生物活性正在进行中。
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| 关 键 词： | 芳酰氨基硫脲 2H－四唑 合成 乙酰基 |
Synthesis of 1-[5-(4-nitrobenzyl)-2H- tetrazol-2-acetyl]-4 aroylthiosemicarbazides |
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| Sun Le,Wang Shaobing,Zhang Yan,Zhang Ziyi.Synthesis of 1-[5-(4-nitrobenzyl)-2H- tetrazol-2-acetyl]-4 aroylthiosemicarbazides[J].Journal of Lanzhou University(Natural Science),1998,34(3):77-81. |
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| Authors: | Sun Le Wang Shaobing Zhang Yan Zhang Ziyi |
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| Abstract: | Ten novel 1-5-(4-nitrobenzyl)-2H- tetrazol-2-acetyl]-4 aroylthiosemicarbazides have been synthesized by the condensation of 5 (4 nitrobenzyl) 2H tetrazol 2 acylhydrazide with various aroylisothiocyanates. The structures of these compounds have been determined by elemental analysis, IR,, 1H NMR and MS, and their biological activities are now under testing. |
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| Keywords: | aoylthiosemicarbazides 2H tetrazole synthesis |
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