| 不同取代2',4'-二羟基查尔酮的合成 |
| |
| 引用本文： | 赵莹,张建平,李彤,梁力曼,王月辉,赵永光.不同取代2',4'-二羟基查尔酮的合成[J].河北科技师范学院学报,2014(2):27-30. |
| |
| 作者姓名： | 赵莹 张建平 李彤 梁力曼 王月辉 赵永光 |
| |
| 作者单位： | 河北科技师范学院化学工程学院,河北秦皇岛066600 |
| |
| 基金项目： | 河北省高等学校科学技术研究青年基金项目（项目编号：QN20131095）部分内容 |
| |
| 摘 要： | 以间苯二酚和苯甲醛为起始原料,经两步加热回流合成法合成了几种2',4'-二羟基查尔酮。结果表明,以对甲苯磺酸为催化剂,其用量为反应物总质量的15%,冰醋酸为溶剂,温度为90℃,合成的取代查尔酮化合物,产率为61.51%~74.96%。
|
| 关 键 词： | 查尔酮 ' '-二羟基查尔酮 合成 |
Synthesis of Substituted 2＇,4＇-Dihydroxychalcone |
| |
| ZHAO Ying,ZHANG Jian-ping,LI Tong,LIANG Li-man,WANG Yue-Hui,ZHAO Yong-guang.Synthesis of Substituted 2＇,4＇-Dihydroxychalcone[J].Journal of Hebei Normal University of Science & Technology,2014(2):27-30. |
| |
| Authors: | ZHAO Ying ZHANG Jian-ping LI Tong LIANG Li-man WANG Yue-Hui ZHAO Yong-guang |
| |
| Institution: | ( College of Chemistry Engineering, Hebei Normal University of Science ＆ Technology, Qinhuangdao Hebei ,066600, China) |
| |
| Abstract: | Substituted 2＇,4＇-dihydroxy chalcones were synthesized by two step heating reflux method with starting materials of resorcinol and benzaldehyde.The yield of 2＇,4＇-dihydroxy chalcones were 61.51% ~ 74.96%in the condition of glacial acetic acid as solvent,p-toluene sulfonic acid as catalyst（ the dosage is 15% of the total mass of reactants）,and the reaction temperature at 90 ℃. |
| |
| Keywords: | chalcone 2 4-Dihydroxychalcone synthesis |
| 本文献已被 CNKI 维普 等数据库收录！ |
|
