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| 微波辐射法合成1-苯甲酰基-3-对甲基苯基硫脲 | |
| 引用本文： | 杜文虎,王清,王伟凤,韦长梅.微波辐射法合成1-苯甲酰基-3-对甲基苯基硫脲[J].淮阴师范学院学报(自然科学版),2009,8(2):160-162. |
| 作者姓名： | 杜文虎 王清 王伟凤 韦长梅 |
| 作者单位： | 1. 淮阴师范学院,化学系,江苏,淮安,223300;南京工业大学,理学院,江苏,南京,210009 2. 淮安市排水监管中心,江苏,淮安,223000 3. 淮阴师范学院,化学系,江苏,淮安,223300 |
| 基金项目： | 江苏省高校自然科学基金资助项目 |
| 摘 要： | 微波辐射法具有反应时间短、产率高、副反应少、易于分离提纯等优点.本文采用微波辐射法合成了1-苯甲酰基-3-对甲基苯基硫脲,通过元素分析、IR和1HNMR对其结构进行了表征,并从微波功率的选择和反应时间两方面优化了反应条件,结果表明:微波功率60 W,反应10 min收率最高. |
| 关 键 词： | 微波 合成 酰基硫脲 1-苯甲酰基-3-对甲基苯基硫脲 |
Synthesis and Characterization of 1-benzoyl-3-(p-tolyl)thiourea under Microwave Irradiation |
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| DU Wen-hu,WANG Qing,WANG Wei-feng,WEI Chang-mei.Synthesis and Characterization of 1-benzoyl-3-(p-tolyl)thiourea under Microwave Irradiation[J].Journal of Huaiyin Teachers College(Natrual Science Edition),2009,8(2):160-162. | |
| Authors: | DU Wen-hu WANG Qing WANG Wei-feng WEI Chang-mei |
| Institution: | 1.Department of Chemistry;Huaiyin Teachers College;Huaian Jangsu 223300;China;2.College of Science;Nanjing University of Technology;Nanjing Jiangsu 210009;China;3.Huaian Draining Water Regulatory Center;Huaian Jiangsu 223300;China |
| Abstract: | Organic synthesis reactions under microwave irradiation had many merits with excellent yield,short time,simple operation,less secondary reaction and easily separated and purified.The compound of 1-benzoyl-3-(p-tolyl)thiourea have been synthesized in the paper,and the structure of the compound was confirmed by elemental analysis,IR and 1H NMR.In addition,the optimum reaction conditions were obtained according to microwave power and reaction time.The result indicate that the yield of product is tiptop when th... |
| Keywords: | microwave synthesis acylthiourea 1-benzoyl-3-(p-tolyl)-thiourea |
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