| 一类带有吡唑基官能团的新型噻吩甲酸类配体的合成和表征 |
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| 引用本文： | 徐文佳,洪芳,孙丽,张卫民,冯宇.一类带有吡唑基官能团的新型噻吩甲酸类配体的合成和表征[J].广西民族学院学报(自然科学版),2012(3):93-95,99. |
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| 作者姓名： | 徐文佳 洪芳 孙丽 张卫民 冯宇 |
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| 作者单位： | [1]广西民族大学化学化工学院,广西南宁530006 [2]广西林产化学品开发与应用工程重点实验室,广西南宁530006 |
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| 基金项目： | 基金项目：广西自然科学基金项目（2010GXNSFC013006）;广西民族大学学校引进人才科研启动项目（2008QD021）;广西科学研究与技术开发计划项目（桂科能0992028--13）. |
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| 摘 要： | 以2-噻吩甲醛和3-噻吩甲醛为原料经过溴代、氧化、肼取代、环合、水解等多步反应合成三种新型吡唑-噻吩类有机配体：5-（3，5-二甲基-1-吡唑基）-噻吩一2-甲酸、2-（3，5-二甲基-1-吡唑基）-噻吩-3-甲酸及2，5-双（3，5-二甲基-1-吡唑基）-噻吩-3-甲酸，并对其结构进行了表征．
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| 关 键 词： | 噻吩衍生物 合成 水解 |
Synthesis and Characterization of New Sorts of Heterocydic Ligands Which Having 1H-Pyrazol-l-yl-Tiophene-Carboxylic Acids |
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| XU Wen-Jia,HONG Fang,SUN Li,ZHANG Wei-Min,FENG Yu.Synthesis and Characterization of New Sorts of Heterocydic Ligands Which Having 1H-Pyrazol-l-yl-Tiophene-Carboxylic Acids[J].Journal of Guangxi University For Nationalities(Natural Science Edition),2012(3):93-95,99. |
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| Authors: | XU Wen-Jia HONG Fang SUN Li ZHANG Wei-Min FENG Yu |
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| Institution: | 1 .College of Chemistry and Ecological Engineering, GuangXi University for Nationalities , Nanning 530006, China; 2. GuangXi Key Laboratory of Chemistry and Engineering of Forest Products , Nanning 530006, China) |
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| Abstract: | Through bromo-substitution, oxidation, diazanyl substitution, cyclocondensauon , nyarolysis reactions , three novel organic heterocydic ligands have been synthesised by thiophene-2-carbaldehyde and thiophene-3-carbaldehyde as materials, and their chemical structures were characterized by IR,1H NMR,13C NMR and MS . |
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| Keywords: | carboxylic acid synthesis hydrolysis |
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