| N—二茂铁烷基氨基醇的正相和反相薄层色谱法 |
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| 引用本文： | 宝凤荣,吴晓萍.N—二茂铁烷基氨基醇的正相和反相薄层色谱法[J].内蒙古大学学报(自然科学版),1989,20(3):362-366. |
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| 作者姓名： | 宝凤荣 吴晓萍 |
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| 作者单位： | 内蒙古大学化学系，内蒙古大学化学系，内蒙古大学化学系，内蒙古大学化学系，内蒙古大学化学系 |
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| 摘 要： | 用硅胶G作吸附剂,以二氯甲烷-正己烷-丙酮(2:1:2),环己烷-1,4-二氧六环(9:7),石油醚-1,4-二氧六环(5:4)作展开剂;用石蜡油浸渍硅藻土G板,以甲醇-水(12:9)为展开剂,对19个N-二茂铁烷基氨基醇分别作正相和反相薄层色谱分离,均得到良好的分离效果。
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| 关 键 词： | N-二茂铁烷基氨基醇 薄层色谱 反相薄层色谱 |
Thin-Layer and Reversed Phase Thin-Layer Chromatography of N-Ferrocenylalkyl Amino-alcohol |
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| Bao Fengrong Wu Xiaoping Wang Yanfei Luo Meihua Li Fengze.Thin-Layer and Reversed Phase Thin-Layer Chromatography of N-Ferrocenylalkyl Amino-alcohol[J].Acta Scientiarum Naturalium Universitatis Neimongol,1989,20(3):362-366. |
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| Authors: | Bao Fengrong Wu Xiaoping Wang Yanfei Luo Meihua Li Fengze |
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| Institution: | Department of Chemistry |
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| Abstract: | Nineteen N-ferrocenylalkyl amino-alcohol have been separated by TLC using silica gel as absorbent, dichloromethane: n-hexane: acetone(2: 1: 2), cyclohexane: p-dioxane(9: 7),or petroleum ether: P-dionane(5: 4) as developer, and by reversed phase TLC using plates of Kieselguhr G layers impregnated with the paraffin oil, methyl alcohol: water(12: 9) as developer. The effect of Separation is better. |
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| Keywords: | N-Ferrocenylalkyl amino alcohol Thin-Layer chromatography Reversed phase TLC |
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