| 氨基甲酸乙酯的合成 |
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| 引用本文： | 李伍林,汪新亮,周平春.氨基甲酸乙酯的合成[J].咸宁学院学报,2005,25(3):99-100. |
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| 作者姓名： | 李伍林 汪新亮 周平春 |
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| 作者单位： | 1. 咸宁学院,药学院,湖北,咸宁,437100
2. 嘉鱼县成人中专,湖北,嘉鱼,437200 |
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| 摘 要： | 氨基甲酸乙酯是重要的化工原料，将尿素与无水乙醇混合，以浓H2S04为催化剂，回流72h，产生大量白色NH4HSO4固体，趁热过滤，除去NH4HSO4固体，滤液常压蒸馏，蒸出多余的乙醇，得到一种胶状物，将胶状物用热的石油醚洗涤、抽滤，得到白色、针状固体氨基甲酸乙酯，产率33．7％。
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| 关 键 词： | 氨基甲酸乙酯 合成方法 |
| 文章编号： | 1006-5342（2005）03-0099-02 |
| 收稿时间： | 03 28 2005 12:00AM |
| 修稿时间： | 2005-03-28 |
Synthesis of Ethyl Carbonate Pharmacology |
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| LI Wu-lin,WANG Xin-liang,ZHOU Ping-chun.Synthesis of Ethyl Carbonate Pharmacology[J].Journal of Xianning College,2005,25(3):99-100. |
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| Authors: | LI Wu-lin WANG Xin-liang ZHOU Ping-chun |
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| Abstract: | Ethyl carbonate is an important material of chemical industry. Mixing up urea with absolute ethyl alcohol, with thigh H_2SO_4 as catalyst, for 72 hours' reflux, will produce a great amount of white solid NH_4HSO_4. Filter while it is hot; eliminate solid NH_4HSO_4; distil under the normal pressure and extra alcohol will be distilled; as a result, a kind of collide will be obtained. After it is cleansed with petrol-ether and filtered, a kind of white, needled solid-ethyl carbonate will be obtained. It's yield rate is 33.7%. |
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| Keywords: | Ethyl carbonate Synthetic method |
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