| 棉籽油脂肪酸正丁基酰胺的合成及表征 |
| |
| 引用本文： | 陈玉成,陈炜,侯桂锋,陈青青,范培珠.棉籽油脂肪酸正丁基酰胺的合成及表征[J].厦门理工学院学报,2012(1):52-55,60. |
| |
| 作者姓名： | 陈玉成 陈炜 侯桂锋 陈青青 范培珠 |
| |
| 作者单位： | 福建师范大学福清分校生物与化学工程系,福建福清350300 |
| |
| 基金项目： | 福建省教育厅B类项目（JB11185）;厦门市科技计划指导性项目（3502220109013）;厦门市科技计划项目（3502220103035） |
| |
| 摘 要： | 以棉籽油脂肪酸和正丁胺为原料合成了棉籽油脂肪酸正丁基酰胺．通过正交试验，确定其合成的最佳工艺条件：反应温度为125℃、反应时间为3．0h、催化荆用量为1．5％、投料比（棉籽油脂肪酸与正丁胺摩尔比）10：7．在优化反应条件下正丁胺的转化率达92．45％，通过红外光谱进行结构表征，确定反应产物为目标产物．
|
| 关 键 词： | 表面活性剂 棉籽油脂肪酸 正丁胺 合成 |
Synthesis and Characterization of Cottonseed Oil Fatty Acid Butylamide |
| |
| CHEN Yu-cheng,CHEN Wei,HUO Gui-feng,CHEN Qing-qing,FAN Pei-zhu.Synthesis and Characterization of Cottonseed Oil Fatty Acid Butylamide[J].Journal of Xiamen University of Technology,2012(1):52-55,60. |
| |
| Authors: | CHEN Yu-cheng CHEN Wei HUO Gui-feng CHEN Qing-qing FAN Pei-zhu |
| |
| Institution: | ( Department of Biological and Chemical Engineering, Fuqing Branch of Fujian Normal University, Fuqing 350300, China) |
| |
| Abstract: | Fatty acid butylamide was synthesized with fatty acid from cottonseed oil and butylamine used as raw materials in this article. Synthetic conditions of fatty acid butylamide were researched through orthogonal experiment. The optimum technological conditions were as following： reaction temperature 125 ~C, reaction time 3.0 h, amount of catalyst 1.5%, molar ratio of fatty acid and butylamine 10： 7. Conversion rate of butylamine can reach 92.45% under optimum conditions. The＇structure of product was confirmed by Fourier transform infrared spectrometer（FTIR） for identifvin~ the product as the taruet object. |
| |
| Keywords: | surfactant cottonseed oil fatty acid butylamine synthesis |
| 本文献已被 CNKI 维普 等数据库收录！ |
