| 5-氨基-3-氰基-1-(2,6-二氯-4-三氟甲苯基)吡唑衍生物的合成及其光物理性能 |
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| 引用本文： | 陈连清,陈贵娣,程国森,吴松.5-氨基-3-氰基-1-(2,6-二氯-4-三氟甲苯基)吡唑衍生物的合成及其光物理性能[J].中南民族大学学报(自然科学版),2011,30(1):5-8,12. |
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| 作者姓名： | 陈连清 陈贵娣 程国森 吴松 |
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| 作者单位： | 中南民族大学,化学与材料科学学院,武汉,430074 |
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| 基金项目： | 国家自然科学基金资助项目，湖北省自然科学基金资助项目 |
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| 摘 要： | 为探索芳基吡唑衍生物的合成及其光物理性能,以2,6-二氯-4-三氟甲基苯胺为原料,经重氮化、环化缩合制得了3种5-氨基-3-氰基-1-(2,6-二氯-4-三氟甲苯基)吡唑(NH2APC)衍生物,对这些化合物进行了FT-IR、NMR、MS和元素分析等表征,并测试了化合物的紫外、荧光光谱,探讨了其光物理性能.结果表明:通过改进NH2APC的合成方法,降低了合成各步反应成本且收率高,目标化合物光物理性能良好.
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| 关 键 词： | 芳基吡唑衍生物 合成 表征 光物理性能 |
Synthesis and Photophysical Properties of 5-Amino-1-(2, 6-Dichloro-4-Trifluoromethyl-Phenyl)-1H-Pyrazole-3-Carbonitrile Derivatives |
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| Chen Lianqing,Chen Guidi,Cheng Cuosen,Wu Song.Synthesis and Photophysical Properties of 5-Amino-1-(2, 6-Dichloro-4-Trifluoromethyl-Phenyl)-1H-Pyrazole-3-Carbonitrile Derivatives[J].Journal of South-Central Univ for,2011,30(1):5-8,12. |
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| Authors: | Chen Lianqing Chen Guidi Cheng Cuosen Wu Song |
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| Institution: | Chen Lianqing,Chen Guidi,Cheng Guosen,Wu Song (College of Chemistry and Materials Science,South-Central University for Nationalities,Wuhan 430074,China) |
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| Abstract: | In order to exploring the synthesis and photophysical properties of aryl pyrazole derivatives,three series of derivatives of 5-Amino-1-(2,6-dichloro-4-trifluoromethyl-phenyl)-1H-pyrazole-3-carbonitrile were synthesized,using 2,6-dichloro-4-trifluoromethyl-phenylamine as the starting materials,the structures of these derivatives have been fully characterized by FT-IR,NMR,MS and element analysis.The electronic absorption and fluorescent properties of these compounds showed good photophysical properties.Their ... |
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| Keywords: | aryl pyrazole derivatives synthesis characterization photophysical properties |
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