| 5-硝基糠醛缩胺类化合物的合成 |
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| 引用本文： | 刘浪,李鸿波,马昌鹏,陈凯.5-硝基糠醛缩胺类化合物的合成[J].云南大学学报(自然科学版),2012,0(3):329-332,347. |
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| 作者姓名： | 刘浪 李鸿波 马昌鹏 陈凯 |
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| 作者单位： | 西南科技大学材料科学与工程学院 |
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| 基金项目： | 西南科技大学研究生创新基金资助项目(11ycjj10) |
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| 摘 要： | 以糠醇为原料,经酯化,硝化,水解,氧化制得关键中间体5-硝基糠醛,总收率51%;再与胺类化合物反应合成了一系列5-硝基糠醛缩胺类化合物,收率71%~89 %.产物及中间体经IR,1H NMR,MS确证结构.
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| 关 键 词： | 5-硝基糠醛 5-硝基糠醛缩胺类化合物 有机合成 |
Synthesis of 5-nitro-furfuralimine compounds |
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| LIU Lang,LI Hong-bo,MA Chang-peng,CHEN Kai.Synthesis of 5-nitro-furfuralimine compounds[J].Journal of Yunnan University(Natural Sciences),2012,0(3):329-332,347. |
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| Authors: | LIU Lang LI Hong-bo MA Chang-peng CHEN Kai |
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| Institution: | (School of Material Science and Engineering,Southwest University of Science and Technology,Mianyang 621010,China) |
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| Abstract: | The key intermediate of 5-nitro-furfuraldehyde was synthesized from furfuryl alcohol by esterification,nitration,hydration and oxidation,the total yield was 51%.A series of 5-nitro-furfuralimine compounds were prepared form 5-nitro-furfuraldehyde with various amines in the yield of 71%—89 %.The structures of the products and intermediate were confirmed by IR,1H NMR and MS. |
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| Keywords: | 5-nitro-furfuraldehyde 5-nitro-furfuralimine compounds synthesis |
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