| 氧化亚锡催化合成乙酸呋喃甲酯的研究 |
| |
| 引用本文： | 陈小原,陈海燕,梁明辉,游志新.氧化亚锡催化合成乙酸呋喃甲酯的研究[J].吉首大学学报(自然科学版),2000,21(4):56-58. |
| |
| 作者姓名： | 陈小原 陈海燕 梁明辉 游志新 |
| |
| 作者单位： | (吉首大学生命科学与化学学院,湖南 吉首 416000 ) |
| |
| 基金项目： | 湖南省教育厅自然科学基金资助项目(99C70) |
| |
| 摘 要： | 研究了碱浓度对糠醛歧化反应中醇收率的影响,得出了最佳碱浓度,并将收率由65%提高到75.9%.采用固体催化剂氧化亚锡催化合成乙酸呋喃甲酯,分析了催化剂用量、反应温度、醇酸比对酯收率的影响,得出最佳反应条件,酯收率为80.9%.
|
| 关 键 词： | 糖醛 呋喃甲醇 氧化亚锡 乙酸呋喃甲酯 合成 |
| 文章编号： | 1007-2985(2000)04-0056-03 |
| 修稿时间： | 2000年8月25日 |
Synthesis of Furfurl Acetate By Stannous Oxide Catalyst |
| |
| CHEN Xiao-yuan,CHEN Hai-yan,LIANG Min-fei,YOU Zhi-xin.Synthesis of Furfurl Acetate By Stannous Oxide Catalyst[J].Journal of Jishou University(Natural Science Edition),2000,21(4):56-58. |
| |
| Authors: | CHEN Xiao-yuan CHEN Hai-yan LIANG Min-fei YOU Zhi-xin |
| |
| Institution: | ( Life Sciences and Chemistry College, Jishou University, Jishou,416000,Hunan China) |
| |
| Abstract: | This paper studied the influence of alcohol yield caused by alkoli consistence in furfural cannizzaro reaction,finally got the most accurate alkali consistence as 33% and increased the alcohol yield from 65.5% to 75.9%.By using solid catalyst stannous oxide esterification we synthesized furfurl acetate and studied the influence of ester yield caused by alcohol/acid mole ratio,the quantity of catalyst.Finally we got the best reaction condition in which ester yield was 80.9%. |
| |
| Keywords: | furfural furfuryl alcohol stannous oxide furfurl acetate synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《吉首大学学报(自然科学版)》浏览原始摘要信息 |
| 点击此处可从《吉首大学学报(自然科学版)》下载免费的PDF全文 |
