刺玫果提取物胶囊定性定量研究

建立刺玫果提取物胶囊的定性鉴别和含量测定方法.采用薄层色谱法对刺玫果提取物胶囊进行了定性分析;采用紫外-可见分光光度法,建立了刺玫果提取物胶囊总黄酮的含量测定方法;采用高效液相色谱法,建立了刺玫果提取物胶囊中金丝桃苷的含量测定方法.结果表明建立的薄层色谱鉴别方法,荧光斑点清晰,阴性无干扰;芦丁在4.0~48.0μg/mL(r=0.9996),金丝桃苷在0.192~1.152μg(r=0.9999)线性关系良好;芦丁平均回收率100.05%,RSD为1.40%(n=6);金丝桃苷平均回收率99.39%,RSD为0.66%(n=6).建立的薄层鉴别方法专属性高,含量测定方法具有良好的精密度,结果准确可靠,可用于刺玫果提取物胶囊的质量控制.     

微波消解-石墨炉原子吸收光谱法测定胶囊的铬

研究了以微波消解仪消解处理、石墨炉原子吸收分光光度计测定胶囊中铬含量的方法。结果表明加标回收率为93.4%~104.8%,检出限为0.0258μg/L。     

聚乳酸／双亲性葡聚糖中空纳米囊泡包载亲水性药物及释放

亲水性药物包载是缓释纳米微粒制备的难点，通过共透析胆固醇改性葡聚糖和聚乳酸得到表面多糖修饰的中空纳米囊泡，在透析过程中以氯化钆溶液代替水相，所得纳米囊通过透射电子显微镜观察和热失重分析测试，证明氯化钆可包载于中空纳米囊泡的亲水性内核，且在纳米囊泡壁形成微孔道．将此纳米囊对亲水性药物头孢拉定反透析，药物通过微孔道扩散进入内核得到载药纳米囊．药物释放研究表明，纳米囊泡使亲水性药物持续释放24h以上，具有缓慢释放的特性．     

贵州红山茶(Camellia kweichouensis)花和果实的形态学研究

运用宏观形态学的方法对贵州红山茶的花和果实形态进行了系统的研究,并分析了其原始性状与进化特征.结果表明贵州红山茶是属于复合体类型.     

用HPLC法测定根痛平胶囊中芍药苷的质量比

对根痛平胶囊中的君药白芍的有效成分芍药苷的质量比测定方法进行了研究;采用高效液相色谱法测定根痛平胶囊中芍药苷的质量比;测得根痛平胶囊中芍药苷质量比为1.284 9 mg/粒;采用高效液相色谱法测定根痛平胶囊中芍药苷的质量比可作为根痛平胶囊的定量标准,测定方法简便、准确、可靠、重现性好.     

HPLC法测定胆立清胶囊中芍药苷的含量

报道了中药复方中白芍、赤芍和丹皮同时含有芍药苷时的处理方法，方法要靠，重现性良好，回收率符合要求。     

建立人脑膜瘤动物模型的实验研究

为建立人脑膜瘤的动物模型，我们从临床上中获得的５例脑膜瘤手术标本移植于裸鼠肾包膜下和皮下，结果肾包膜下移植的１２只裸鼠有１１只获得肿瘤生长，成功率９１．７％。肿瘤的体积在４－１０周可达原体积的２－３倍。血管形成很明显，并随肿瘤体积不断增大而数目增多，管径增粗。病理切片示移植于裸鼠的肿瘤与原外科手术切除的标本在形态学上一致，保持了人类脑膜瘤的形态特点。     

Reproductive phenology and pre‐dispersal seed‐feeding in Protium tovarense (Burseraceae), with a description of the first known phytophagous “Bracon” species (Hymenoptera: Braconidae: Braconinae)

The reproductive phenology of the cloud forest tree Protium tovarense (Burseraceae) is analysed for one population in northern Venezuela. Reproductive phenophases were monitored using both long‐term(21 years) and detailed short‐term (4 years) surveys of flower and fruit set. The reproductive phenology of this tree varies, with periods in which the species behaves as a supra‐annual reproducer, and other periods in which it reproduces annually, at the end of the rainy season. Marked spatial variation in reproductive condition was also observed, with subpopulations separated by less than 2 km showing contrasting phenological stages. Larval infestation of seeds by a braconid wasp was observed for a period of 1 year and is described. This wasp, the first obligately phytophagous species of Braconinae, is described as Bracon phytophagus Quicke sp. n. Percentage fruit infestation by this wasp was relatively high (50–60%) during the entire period (～10 months) of fruit development. The larval stages are described and illustrated, and compared with those of other phytophagous Ichneumonoidea. DNA sequencing of wasp colour variants provided no indication that multiple species were involved. Two related braconine species described in the genus Iphiaulax are transferred to Bracon, hence, B. flavipalpisimus replacement name (Szépligeti) ( = Iphiaulax flavipalpis Szépligeti, 1901 Szépligeti, G v. 1901. Tropische Cenocoeliden und Braconidae aus der Sammlung des Ungarischens National‐Museums.. Természetrajzi Füzetek, 24: 353–402.  [Google Scholar] not B. flavipalpis Thomson, 1892) and B. glabrescens (Szépligeti) n. comb. ( = Iphiaulax glabrescens Szépligeti, 1901 Szépligeti, G v. 1901. Tropische Cenocoeliden und Braconidae aus der Sammlung des Ungarischens National‐Museums.. Természetrajzi Füzetek, 24: 353–402.  [Google Scholar]). Evolutionary routes to phytophagy in braconid wasps and hypothetical scenarios in which this plant–seed predator interaction can be maintained are discussed.     

混凝防渗墙在涵管上的施工浅析

病险水库除险加固中,垂直防渗墙在涵管上的施工是难点。采用橡胶充气胶囊在涵管内予留防渗墙施工尺寸,上下游封堵涵管,防渗墙泥浆槽在两胶囊之间通过。待防渗墙初凝后,放空胶囊,在墙上重新打孔,接通涵管。既可以解决施工中漏浆、漏水的问题,又能达到缩短工期、不误用水的目的,具有推广价值。     

调血保肾胶囊治疗小儿过敏性紫癜肾炎的临床研究

目的探讨调血保肾胶囊为主配合西药治疗小儿过敏性紫癜肾炎的疗效。方法将门诊和住院患儿284例随机分为观察组、对照组,观察组用调血保肾胶囊为主配合西药治疗,对照组采用常规治疗,对比疗效。结果观察组156例,完全缓解96例,占61.54%,总有效141例,总有效率达90.38%;对照组128例,完全缓解63例,占49.22%,总有效102例,总有效率达79.69%。2组比较P<0.05,证实调血保肾胶囊治疗小儿过敏性紫癜的肾炎,具有较好的疗效。