痕量PBBs/PBDEsGC/MS分析法中PCB及其衍生物干扰消除方法

电子电气产品中痕量阻燃剂聚溴联苯/聚溴联苯醚(PBBs/PBDEs)的检测通常采用气相色谱/质谱(GC-MS)联用法,但该法是建立在持久性污染物多氯化苯/多氯化萘(PCBs/PCNs)基础上,因此此类物质干扰不可避免。为了解决此类问题,提出了2种解决方法:1)阴离子化学电离-气相色谱/质谱联用法(GC/MS-NICI)和电子轰击-气相色谱/质谱联用法(GC/MS-EI)联合使用;2)以YMC ODS-C18为载体,基质固相分散法(MSPD)吸附分离。结果显示,前者可以同时洞察聚溴联苯和联苯醚的分子链断裂后阴离子碎片[Br]-,[HBr2]-和分子链段碎片[M+2]+,[M+4]+,[M+6]+,[M+8]+的滞留峰,增加了对溴系阻燃剂的选择性。后者可以有效分离多种多氯化苯与聚溴联苯醚的色谱峰,这为溴系阻燃剂气相色谱/质谱联用分析法中多氯化苯及其衍生物干扰提供了新的解决方法。采用此方法对8类电子电气产品中10种聚溴联苯醚和多氯化苯进行加标回收实验及精密度分析,回收率在60%～98%,相对误差在9.5%以内,符合国际电工委员会(IEC)对溴系阻燃剂检测精度要求,说明方法具有较高的可靠性,也为我国电子电气业更好遵守...     

并行组合扩频超宽带系统的跳时多址接入性能

针对前期提出的并行组合扩频超宽带通信系统,采用跳时多址接入方式,通过分析文中系统的误码性能和多用户接入数量,对其多址性能进行研究.仿真结果表明:跳时多址接入方式的采用改善了并行组合扩频超宽带通信系统的多址性能,大幅提高了系统容量;在大信噪比环境中,该采用跳时多址接入的系统工作在5个干扰用户条件下的误码性能仍比在单用户条件下工作的传统超宽带通信系统有较大的提高.进一步分析了该多址系统可容纳的用户数量,认为较多用户干扰时可以考虑采用新的跳时码减少脉冲间发生碰撞的概率,以降低多用户干扰.     

番茄CDT2同源基因RNA干涉载体的构建及遗传转化研究

真核生物CDT2是CUL4-DDB1 E3泛素复合体的组成部分,在细胞周期调控、DNA复制与损伤修复中起到重要作用.本研究克隆了番茄CDT2同源基因片段并构建了CDT2基因RNA干涉植物表达载体pBI121-CDT2-RNAi.通过根癌农杆菌介导转入番茄子叶,经组织培养成功获得转基因植株.半定量RT-PCR分析显示,转基因植株叶片内CDT2的表达量明显低于野生型植株.转基因植株叶片叶绿素含量比野生型明显升高.该研究结果揭示番茄CDT2基因的功能做出了新的尝试.     

奈奎斯特滤波器设计

本文研究了非线性相位响应的奈奎斯特第一准则滤波器（NF1′s）的设计方法，在此理论基础上，提出了一种在有或无匹配滤波器情况下，奈奎斯特第一准则通用滤波器的设计、转换方法。     

基于卫星干扰源定位系统的星历获取方法

在干扰源定位系统对目标实现定位时,需要知道卫星的位置、速度,由于网上星历更新速度不很及时,导致有时获取的卫星星历误差较大,因此需要通过测量获取卫星的星历.在卫星动力学方法的基础上,不添加任何硬件设备的条件下,研究了基于卫星干扰源定位系统星历获取方法,并对这种方法进行了仿真分析,对星历的精度进行评估.仿真结果表明这种方法获取的卫星星历优于从网站下载的卫星星历,满足定位系统的需求.     

镶嵌铜多孔铝膜透射光谱曲线中干涉现象的研究

用阳极氧化的方法制备了阳极氧化铝膜,向其孔中镀入了铜,然后利用UV-3101PC型分光光度计进行了透射光谱测试.实验结果表明,在其可见光和近红外光波段的透射曲线中有明显的振荡现象.利用Maxwell-Garnett理论,分析了这种振荡现象产生的原因,从理论上说明了这种振荡现象是由薄膜干涉引起的,最后提出了用冷杉胶将多孔铝膜胶合在两BaF2窗口的方法,有效消除了透射光谱曲线中的干涉效应.     

Complexity-reduced ICI cancellation for OFDM system over doubly-selective channels

In doubly-selective fading wireless channel,the conventional orthogonal frequency division multi-plexing(OFDM)receivers for inter-carrier interference(ICI)compensation require extensive computa-tions.To obtain an effective balance between performance and complexity,the whole channel responsematrix was decomposed into a sequence of submatrix,and then a novel equalizer based on minimum meansquare error(MMSE)criterion was presented to combat the ICI.Furthermore,a simple ordering-baseddecision-feedback equa...     

Distributed link scheduling method with physical interference model in wireless multi-hop networks

To further increase the throughput of wireless multi-hop networks,a distributed scheduling method is proposed,which takes physical interference model into account.It is assumed that nodes in the network can perform physical carrier sensing,and the carrier sensing range can be set to different values.In the traditional carrier sensing mechanism,the carrier sensing range is computed under the protocol interference model,which is not accurate.Here the optimal carrier sensing range with physical interference model is achieved.Each sending node implements the distributed approach in three phases at each time slot,and all the concurrent transmissions are interference free.Good performance can be achieved under this scheduling approach.The approximation ratio of the distributed method to the optimal one is also proved.     

Concurrent transmission with minimal SR-pair interference in WiMAX mesh networks

Performance of wireless mesh networks can be greatly improved by spatial reuse (SR), therefore, lots of algorithms have been proposed to maximize the number of concurrent transmissions. However, most methods only considered the interference brought by the sender nodes. In this paper, we study the interference model in WiMAX mesh networks and propose a minimal SR-pair interference model to perform concurrent transmissions in both uplink and downlink directions. Simulation results show that our model is more efficient and stable, i.e., it increases the number of concurrent transmissions and its performance is constant and independent of transmission directions. Biography: XIONG Qing(1978–), male, Ph. D., research direction: wireless mesh networks.