Occurrence of 3-epi-22-deoxy-20-hydroxyecdysone and its phosphoric ester in diapause eggs of the silkworm,Bombyx mori

Ecdysteroids in diapause eggs of the silkworm,Bombyx mori, were analyzed using high-performance liquid chromatography (HPLC) combined with radioimmunoassay (RIA). A relatively large amount of an unidentified free ecdysteroid and its phosphoric ester (conjugated form) were detected. These two compounds were isolated by a combination of column chromatography on silicic acid, thin-layer chromatography (TLC), and HPLC using a reverse-phase (RP) column. The purified compounds were identified as 3-epi-22-deoxy-20-hydroxyecdysone (22d20E) and 3-epi-22-deoxy-20-hydroxyecdysone 2-phosphate (22d20E2P) by means of mass spectrometry and nuclear magnetic resonance spectroscopy. to our knowledge, this is the first report of 22d20E and 22d20E2P.     

机载MIMO雷达3-CAP杂波抑制方法

针对机载雷达面临的杂波抑制问题,在考虑阵元误差、通道误差和杂波起伏等误差因素对杂波特性影响的基础上,建立了机载MIMO雷达杂波数学模型,提出了一种基于MIMO雷达体制下的空时自适应新方法——M3-CAP方法。对接收信号进行时域滤波,选取被检测通道与其2个相邻通道为一组,进行自适应处理。该方法通过MIMO技术与3-CAP方法的有效结合,将波形分集的优势扩展到3-CAP方法中,显著提高了雷达系统自由度和杂波协方差矩阵估计精度。通过对不同雷达体制以及不同误差条件下杂波抑制性能的分析比较,结果表明:提出的M3-CAP方法的杂波抑制性能明显优于JDL-GMB、改进的JDL、3-CAP等方法。     

WS~*-闭空间的性质

该文引入了一类包含Ｓ－闭空间的拓扑空间——ＷＳ＊－闭空间,并讨论了它的一些性质,对一些关于Ｓ－闭空间的已知命题,建立或推广得到ＷＳ＊－闭空间的相应命题。     

一种磨茹香气香料——1-辛烯-3-醇的合成与应用研究

从１－戊醇出发,通过卤代反应,格氏反应,制备得到１－辛烯－３－醇。该产品具有愉快的蘑菇香气,可用于食品香精的调配中。     

Cu~(2+)与三磺基四苯基啿卟啉配位反应研究

利用吸收光谱法和直流极谱法研究了Cu~(2+)的还原状态、抗坏态、抗坏血酸浓度及溶解氧对Cu~(2+)与三磺基四苯基卟啉配位反应的影响。结果表明Cu~(2+)与三磺基四苯(?)基四苯基卟啉配位反应的可能机制为抗坏血酸首先将高价铜还原为亚铜,亚铜离子与配位剂生成对氧成对氧敏感的不稳定中间体Cu~(Ⅰ)——三磺基四:苯基卟啉配合物,立即又被溶解氧氧化为Cu(Ⅱ)——Ⅱ)——三磺基四苯基卟啉配合物。     

采用在系统可编程逻辑器件实现HDB3编解码

在系统可编程技术是通信专用集成电路设计的一种最新设计方法,它使得数字电路设计、生产良生革命性的变化。     

SAG法合成钛酸铅纳米晶粒的工艺和结构研究

ＳＡＧ法合成钛酸铅纳米晶粒的工艺和结构研究李永祥刘泽吴冲若（东南大学电子工程系,南京２１００９６）ＰｂＴｉＯ３是应用广泛的铁电和光电材料之－,研究ＰｂＴｉＯ３纳米晶粒的合成技术和电学性能对基础研究和新型复合功能材料研究都有重要意义．作者曾采用Ｓｏｌ...     

地形数据在野战虚拟环境系统中的集成

目的研究在野战战术Ｃ＾３Ｉ系统中利用虚拟现实技术短维图形显示技术仿真战场地形环境。方法介绍了多种地形建模的方法,涉及到由等高线生成三维模型,数字图形处理技术,分表学,细节度表示以及地理信息系统等,并对这些方法进行了比较,分析和改进,结果与结论利用这些方法,比较好地解决了各种情况下野战虚拟环境中地形数据的集成问题,野战虚拟环境系统的设计提供了依据。     

V棱镜法测掺Yb^3＋激光玻璃折射率

用Ｖ棱镜法测量了一类非常用应用前景的掺Ｙｂ＾３＋激光玻璃的折射率,得到了一些有用的数据,对有关掺Ｙｂ＾３＋激光玻璃的研究工作起了一定的辅助作用。     

Leakage of mantle helium from the Liaodong Peninsula, China

The isotopic cumpositions of helium have been investigated in hot spring gases sampled from the Liaodong Peninsula. China. The³He/⁴He ratios range from 0.14 Ra (0.14 times the atmospheric³He/⁴He ratio of 1.40 × 10^-6 to 0.72 Ra.³He/⁴He versus⁴He/²⁰Ne ratios and He contents suggest that a small amount of mantle-derived helium reaches the earth’s surface. Helium iwtope ratios of the hot spring gases show a distribution pattern similar to the regional heat flow values, indicating that the positive thermal anomaly occurring in the rtrea is closely associated with the presence of mantle-derived helium. The observations described above provide some significant evidence that the molten magma originating from partial melting of the upper mantle may have intruded into the continental crust along the activity fault. The coupling of the presence of mantle He and heat flow anomalies to seismic activity in studied region seem to imply that there is an internal relationship between mantle degassing and seismic activity.