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991.
以Waugh结构钼锰杂多酸盐作为催化剂对乙酸异戊酯的合成进行了催化研究.确定了最佳反应条件:醇酸摩尔比为1.646∶1,酸化催化剂用量为0.2 g,带水剂为3 mL甲苯,反应时间63 min左右,选择性100%,转化率达82.70%. 相似文献
992.
Xing Wei ZhongYing Xue AiMin Wu Xiang Wang XianYuan Li Fei Ye Jie Chen Meng Chen Bo Zhang ChengLu Lin Miao Zhang Xi Wang 《科学通报(英文版)》2011,56(4-5):444-448
In this paper, we investigated the dose window of forming a continuous buried oxide (BOX) layer by single implantation at the implantation energy of 200 keV. Then, an improved two-step implantation process with second implantation dose of 3×1015 cm?2 was developed to fabricate high quality separation by implanted oxygen (SIMOX) silicon on insulator (SOI) wafers. Compared with traditional single implantation, the implantation dose is reduced by 18.2%. In addition, the thickness and uniformity of the BOX layers were evaluated by spectroscopic ellipsometry. Defect-free top Si as well as atomic-scale sharp top Si/buried oxide interfaces were observed by transmission electron microscopy, indicating a high crystal quality and a perfect structure of the SOI fabricated by two step implantation. The top Si/BOX interface morphology of the SOI wafers fabricated by single or two-step implantation was also investigated by atomic force microscopy. 相似文献
993.
994.
In this paper,the optimal policy is considered when the buyer faces two supply sources:one is the contract supplier from which the buyer orders over a specific contract period(say,a year) at a pre-agreed price,and the other is the spot market.However,when ordering from the contract supplier,the buyer must fulfill a pre-determined total order quantity,or the so-called definite total order quantity commitment,over the whole contract period.In other words,the commitment secures the buyer a fixed price but obliges him/her a total order quantity over the contract period.Although the spot market gives the buyer more flexibility in terms of order quantities,its prices are volatile.Such a combination of contract and spot procurements is often observed in practice.Within the contract period,there are multiple sub-periods,during each of which the buyer reviews the inventory,issues an individual order,and uses the on-hand inventory to meet the random demand.Thus,in each(ordering) period,the buyer will weigh between the current known spot price(by procuring from the spot market) and a lower future price(by waiting while consuming the remaining commitment).An optimal dual ordering policy is characterized for each period,depending on the on-hand inventory level,the spot price,and the remaining commitment quantity.The optimal policy in each period is also shown to be independent of the contract price.Through a numerical study,the inventory cost is demonstrated to be(1) insensitive to the contract price when the total commitment quantity is lower than the total expected demand over the contract period and(2) non-increasing in the variability of spot prices. 相似文献
995.
A fully discrete implicit Euler upwind finite volume element method is derived and studied for one-dimensional semiconductor
device. Upwind scheme is introduced to deal with the convection-dominated diffusion equations in the semiconductor model.
With different time steps for the electrostatic potential and the other unknown quantities, the computational procedure of
the method is obtained. The local mass conservation laws are preserved under the framework of the upwind finite volume element
schemes. A first-order accuracy in the L
2-norm is proved. Numerical experiments are given to validate the usefulness and efficiency of the method. 相似文献
996.
如何克服高层住宅楼渗漏的质量通病是建筑工程实践和理论界的重大课题.在近几年的高层住宅楼工程施工过程中,建筑工程管理者和技术工作人员高度重视了高层住宅楼工程质量通病的预防,完善和推广了科学有效的高层住宅楼工程防渗漏施工技术措施.本文从高层住宅楼外墙面、外墙窗口、厨房、卫生间及地下室的高层住宅楼工程防渗漏施工完整技术体系入手,介绍了较为有效的控制高层住宅楼工程防渗漏的施工技术措施. 相似文献
997.
Over the past ten years,the enthusiasm to harness small RNA molecules,mainly small interfering RNAs(siRNAs) and microRNA mimics,into therapeutic weapons has never been quenched.However,a major obstacle hindering the clinical application of these small molecules is how to efficiently and precisely deliver siRNAs in vivo into target cells to silence target genes.An international collaborative study led by Song Erwei from the Memorial Hospital of Sun-YatSen University and Wang Jun from Hefei National Laboratory for Physical Sciences at Microscale and School of Life Sciences of University of Science and Tech- 相似文献
998.
讨论了与分类排架相关的倒架、文献增长预测方法、搁板间距确定、书库容书量等问题,介绍了创新型分类排架方法,即通过记录和考察各类目藏书总厚度的增长数据,精确预算预留书架空位,各文种藏书统归为一个序列,构建国家图书馆基藏书库科学的藏书排架体系,其过程包括3个程序:一是测量各类目图书所占搁板长度及预测其增长率,对书库重新规划布局;二是同类书按书型调整搁板间距,重新排架;三是增加架位号书标并录入到OPAC系统中。 相似文献
999.
1000.
豫南大别山区不同海拔高度茶树主要品质成分变化 总被引:1,自引:0,他引:1
采用生化分析和高效液相色谱法,分析了豫南大别山区不同海拔高度茶树的主要成分。结果表明,其主要品质成分的含量为:水浸出物44.52%~46.99%(质量分数,以下同),茶多酚25.49%~30.03%,儿茶素208.49~234.18mg·g-1,氨基酸3.86%~4.81%,可溶性糖4.61%~5.22%,叶绿素1.26~1.98mg·g-1,咖啡碱3.11%~3.72%。综合分析,随海拔高度的升高,茶叶品质逐渐提升,海拔700m处的茶叶品质最佳。 相似文献