IMI及其微生物转化产物5-hydroxy IMI的HPLC分析

研究了烟碱类杀虫剂IMI及其微生物转化产物5-hydroxy IMI的反相高效液相色谱分析方法．采用Zorbox OSD反相柱，水和乙腈（75：25）（v／v）为流动相，流速为1mL／min，检测波长为269nm，IMI和5-hydroxy IMI得到较优分离．在0．5～50mg／L的浓度范围内，两种物质的色谱峰面积和浓度之间呈线性关系，IMI和5-hydroxy IMI的标准工作曲线分别为y=112．23x-1．7775和y=98．039x-17．508；相关系数为0．9999和0．9997．转化产物的样品中IMI和5-hydroxy IMI添加的回收率分别为99．3％和97．4％．     

赛隆-碳化硅系复合材料的合成及其应用

以蜡石和碳黑为原料,通过碳热还原法合成了赛隆-碳化硅系复合材料,将其作为添加剂应用于Al2O3 C系不定形耐火材料中·考察了加热温度对赛隆-碳化硅系复合材料合成过程的影响以及添加赛隆-碳化硅系复合材料对耐火材料性能的影响·研究结果表明,通过向蜡石中添加适量的碳黑,并将蜡石和碳黑的混合物在氮气气氛下加热到1540℃时,可以很容易地合成赛隆-碳化硅系复合材料·通过添加适量的赛隆 碳化硅系复合材料,Al2O3 C系不定形耐火材料的抗氧化性能、抗渣侵蚀性能以及高温抗折强度均得到了明显的改善·     

基于内容的Web集群系统负载均衡策略

Web集群技术解决了Web服务器系统容量问题，其核心思想是负载均衡策略和算法。传统的策略对某些站点类型有效，而不能满足各种类型站点的要求。笔者分析了各种类型站点的负载特点，讨论了负载均衡需要解决的主要问题，提出了一种基于内容的Web集群负载均衡策略和相应的负载均衡算法，并通过仿真实验验证了该策略和算法的有效性。     

新型钢-砼组合结构构件的研究与应用

在工程设计和施工中，对钢管砼及型钢砼-钢筋砼组合的结构提出了许多问题．据此，对这种新型钢-混凝土组合结构构件进行了一系列的试验研究及工程应用．本文是对近8年来研究工作的归纳、总结．其中，提出的较优化的钢筋砼环梁节点、钢加强环节点、钢管砼柱与钢筋砼柱节点、钢骨砼柱与钢筋砼梁节点、钢骨砼柱与组合梁节点及组合梁设计方法、预应力叠层空腹桁架等，都已应用于实际高层建筑中．文中提出的建议，可供工程设计参考使用．     

一种新的二值图像信息隐藏方法

随着数字媒体的普及,人们已经提出了许多在灰度图像和彩色图像中隐藏信息的方法,但是由于随意修改二值图像的像素值容易引起图像质量的明显下降,所以大多数在灰度图像和彩色图像中隐藏信息的方法不能直接应用到二值图像中.本文提出了一种在二值图像中进行信息隐藏的方法.该方法将二值图像分割成大小为2×2的图像块,利用图像块的奇偶性将一条二进制信息嵌入到黑白像素邻近的块中,嵌入1位信息平均修改0.5个像素,具有计算量小、嵌入信息量大、图像质量下降少、安全性高的优点.     

Technical Breakthroughs in the Construction of TGP

1Introduction　TheThreeGorgesProject(TGP)isavitalbackboneprojectinthedevelopingandharnessingoftheYangtzeRiver.Asamulti purposehydro developmentprojectthatcanproducecomprehensivebenefitsmainlyinfloodcontrol,powergenerationandnavigationimprovement,TGPwillexertasignificantimpactonthenationalsocio economicdevelopmentofChinaafteritscompletion .Withthenormalpoollevel (NPL)at1 75m ,thereservoirhasatotalstoragecapacityof39 3billionm3 .Theprojectiscom posedofadam ,twopowerplantsandnavigationfacil…     

Lightning activity on the central Tibetan Plateau and its response to convective available potential energy

Lightning flash activities on the central Tibetan Plateau have been studied by using the satellite-based Lightning Imaging Sensor(LIS)database from January 1998 to July 2002.The lightning activity shows a clear diurnal variation on the central Plateau.The peak lightning activity appears at about 17:00 which is 3 h earlier than that in Jingxhou,Hubei in the same latitude belt nearby,indicating that the lightning activity is a sensitive indicator of solar heating on the Plateau.The lightning discharge is weaker on the Plateau than Jingzhou.Hubei and other low-altitude continental regions because of the lower convective available potential energy(CAPE)on the Plateau.The CAPE on the Plateau is 12 times lower than that in Jingzhou,Hubei,and 20 times lower than that in the sea-level region,such as Guangzhou and Florida.However,the sensitivity of lightning activity to CAPE changes on the Plateau is up to 30 times more sensitive than other prominent low-altitude regions.     

C－isotope composition and significance of the Sinian on the Tarim plate

102 samples of limestones,mudrocks shales and tillites from the Sinian in Kuluketage have been analyzed ,Four formations in the Sinian belong to glacial deposits in which the differences in δ^13C are distinct (-14.7‰- 4.2‰),Distinctly negative δ^13C excursions for three times support the viwe of three glacial deposits in this area suggested by previous authors,except for the durations of them ,δ^13C values are generally positive in the Beiyixi Formation of lower part of the Lower Sinian ,representing probably the rock records of a continental rift related to break-up of the Rodinian supercontinent,There are three times of distinct excursions of δ^13C curve in all strata,The first one is from positive values at the bottom to about -5‰ at the top of the Beiyixi Formation ,The second one,from 0‰-3‰ in the Arletonggou Formation of upper part of the Lower Sinian to -3.4‰---14.4‰ in the Teruiaiken Formation.The third one,from positive values in the Zhamoketi Formation of lower part of the Upper Sinian to negative values in glacial varves at the top of the Hankeerqiaoke Formation.     

A new Euprox from the Late Miocene of Yuanmou,Yunnan Province,China,with interpretation of its paleoenvironment

The Yuanmou Basin of Yunnan Province is a hotspot for the research of early homind evolution and its environmental background.During the implementation of the Program“Research of the Origin and Evolution of Early Man and Its Environmental Baqckground” from 1998 to 2001,a huge quantity of hominoid and mammal fossils were collected.The present report systematically describes an Euprox robustus sp.nov.identified during the recent laboratory work on the collected material.Euprox is a group of earliest cervids with true antlers.The new species is the third one of the genus discovered in China.Judged by its morphologic characteristics,the new species feed on juicy and tender leaves of dicotyledon.It implies that the vegetation of its epoch in the Yuanmou Basin is a kind of southern subtropical evergreen forest and the climate is humid and temperate with evident seasonality.The latter is mostly influenced by the monsoon and secondly by the latitude.     

Inorganic chemical composition and source signature of PM2.5 in Beijing during ACE-Asia period

Aerosol samples for PM2.5 were collected in Beijing for 38 consecutive days from March to April 2001 using an IMPROVE Sampler. Concentrations of 20 elements in PM2.5 were determined using a PIXE method. Results show that the average mineral dust concentration of PM2.5 was 14.6 Ilg/m3 during the observation period. On the sand-dust event days of March 21 and April 10, dust PM2.5 mass concentrations were 62.4 and 54.1 μg/m^3, respectively.These demonstrate that fine particle pollution by dust event in Beijing was very severe. The enrichment factors of S and Cu reached minimums on the dusty days and were high on the non-dusty days. It is considered that enrichment factors of elements in PM2.5, which are associated with human activities, can probably provide an effective method to distinguish local sources from external sources of dust. Factor analysis on the chemical composition in PM2.5 shows that sources of crustal matters, anthropogenic emission, and oil combustion contributed to PM2.5 levels in air in the springtime of 2001 in Beijing.