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991.
XiaoTao Wang YingKui Yang ZhiFang Yang YongGui Liao Wei Zhang XiaoLin Xie 《科学通报(英文版)》2010,55(30):3441-3447
By means of distillation precipitation polymerization, the silica-hybrid particles with polyazobenzene shell (PAzo@SiO2) micro-spheres were prepared with 6-(4-methoxy-4′-oxy-azobenzene) hexyl methacrylate (Azo-M) as monomer, divinylbenzene (DVB) as cross-linker, and ~250 nm vinylated sol-gel silica particles as template. Hollow polyazobenzene microspheres were further developed after selective removal of the silica cores with HF solution. When the content of DVB related to Azo-M is 20 wt%, the acetonitrile is 200 mL, and the polymerization time is 4.5 h, the hollow PAzo microspheres with about 20 nm shell are successfully fabricated. These hollow PAzo microspheres have excellent reversible photoisomerization, and their first-order rate constant of trans-cis isomerization only decreases 11.8% compared with homopolymer of azobenzene (Homo-PAzo). 相似文献
992.
993.
On the basis of the analysis of the system sounding principle, this paper introduced a new type of ionospheric oblique backscattering
sound system, which is based on the pseudo- random noise phase modulated pulse compression. According to the high requirements
of real-time and a large amount of computation and echo characteristics, a high-speed real-time signal processing system was
established and the design of system hardware and software was focused on. The sounding results indicate that the system is
equipped to handle the data fast and has a high degree of software features. It is of great significance for the realization
of fast, real-time ionospheric sounding means.
相似文献
994.
995.
基于金属流动原理,采用显式动力学有限元软件ANSYS/LS-DYNA模拟薄板轧制过程,研究轧制力、摩擦系数、压下率对轧件宽展变化的影响。结果表明,摩擦系数越大,轧件宽展也越大;轧件的最大宽展随着轧制力的增加而增大,轧制力对轧件后端部分宽展影响程度较大;压下率增大,轧件宽展随之增大,轧件各部分宽展的不均匀程度也在增加。 相似文献
996.
在酚醛树脂中直接掺杂三氧化镍粉末,研究氧化镍掺杂量、炭化温度对氧化镍改性树脂热解炭结构和氧化温度的影响。用X射线衍射、拉曼光谱、扫描电镜和综合热分析等手段对氧化镍改性树脂热解炭的石墨化度、显微结构及氧化温度进行表征。结果表明,埋炭条件下掺杂三氧化二镍,450~750℃温度下被逐级还原成一氧化镍和单质镍,其催化热解炭形成晶须、片状或块状结构;氧化镍改性树脂热解炭石墨化度随炭化温度升高和氧化镍掺杂量增加而增高,其氧化温度高于酚醛树脂氧化温度;氧化镍的最佳掺杂量为3%~5%。 相似文献
997.
This research analyzed amino acid sequence similarity between non-self T cell epitopes recognized by mouse antibodies and mouse proteins. Using sequence alignment,we found that only 8 of 1 108 epitopes are highly similar to mouse protein sequences. The result shows that non-self T cell epitopes are not similar or have little similarity to mouse protein sequences. Furthermore,reviewing the related literature,we also found that the eight epitopes would trigger immune responses in some particular environment,which are ignored by T cells in normal condition. The result suggests that no or low-similarity peptide vaccines can reduce the chance of collateral cross-reactions and enhance the antigen-specific immune response to vaccine. 相似文献
998.
In this paper, CdS quantum dots sensitized TiO2 composite powders (QD-CdS/TiO2) were synthesized by impregnating TiO2 powder into CdS sol with different concentrations. X-ray diffraction pattern (XRD) shows the crystal structures of CdS and TiO2 are cubic phase and anatase phase separately in QD- CdS/TiO2 powder samples; the crystal size of CdS in QD- CdS/TiO2 is about 3-7 nm, while TiO2 crystal size is about 20 nm. With increasing CdS content in QD-CdS/TiO2 composite, the UV-Vis absorption spectrum shifted to the longer wavelength lines, exhibiting obvious quantum size effect. The fluorescence intensity of QD-CdS/TiO2 irradiated by blue light is weaker than that of pure CdS. When the molar ratio of CdS and TiO2 is about 1∶2, the QD-CdS/TiO2 powder has the best catalytic properties under visible-light irradiation, and the degradation rate of rhodamine B (RhB) is up to 92.2% within 60 min. 相似文献
999.
In this paper, the joint production and recycling problem is investigated for a hybrid manufacturing and remanufacturing system
where brand-new products are produced in the manufacturing plant and recycled products are remanufactured into as-new products
in the remanufacturing facility. Both the brand-new products and remanufactured products are used to satisfy customer demands.
Returns of used products that are recycled from customers are assumed to be stochastic and nonlinearly price-dependent. A
mathematical model is proposed to maximize the overall profit of the system through simultaneously optimizing the production
and recycling decisions, subject to two capacity constraints — the manufacturing capacity and the remanufacturing capacity.
Based on Lagrangian relaxation method, subgradient algorithm and heuristic algorithm, a solution approach is developed to
solve the problem. A representative example is presented to illustrate the system, and managerial analysis indicates that
the uncertainties in demand and return have much influence on the production and recycling policy. In addition, twenty randomly
produced examples are solved, and computational results show that the solution approach can obtain very good solutions for
all examples in reasonable time. 相似文献
1000.
Well-crystalline CeO2 nanowires were prepared via a surfactant-assisted hydrothermal process. Reaction temperature and reaction time were changed for the determination of
optimal synthesis parameters. The as-obtained products were characterized by X-ray diffraction (XRD), high-resolution transmission
electron microscopy (HRTEM), and field emission scanning electron microscopy (FESEM). The results show that single crystal
CeO2 nanowires with high yield and good uniformity can be obtained hydrothermally at 180°C for 12 h with the aid of 2.0 g surfactant
(polyvinyl pyrrolidone, PVP). The role of PVP was then discussed and a possible growth mechanism was proposed. Moreover, room
temperature photoluminescence (PL) spectra were obtained for these CeO2 nanowires, which are believed to be related to the abundant defects in these nanostructures. 相似文献