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1.
Mn液中Ca溶解量及第3组元的影响   总被引:1,自引:0,他引:1  
用密封容器气液平衡法,测定了Ca在Mn液中的饱和溶解量及第3组元C、Si,Ni,Al,Cr和As对其的影响,得到的Mn液中Ca饱和溶解量与温度的关系式,以及1673K下Mn液中第3组元与钙的活度相互作用系数。  相似文献   

2.
利用阻抑反应测定Mn(Ⅱ)的研究   总被引:3,自引:0,他引:3  
实验证明在pH1.0的HCl-KCl酸性介质中Mn(Ⅱ)阻抑Fe(Ⅲ)催化NaIO4氧化甲苯胺蓝(ToluidineblueC15H16CIN3S)褪色反应是一个新的阻抑反应体系,其阻抑作用和催化反应的速率差与Mn(Ⅱ)含量有线性关系。速率差通过体系在622nm波长处吸光度值的变化求得,从而建立了利用阻抑反应测定Mn(Ⅱ)的新方法。该方法用于井水和自来水中Mn(Ⅱ)测定,获得满意结果。  相似文献   

3.
本研究采用共沉淀方法制备出四种催化剂,CuMn1.36Ox、Ce/CuMn1.36Ox、Au/CuMn1.36Ox和Au-Ce/CuMn1.36Ox。在200℃时,对催化剂进行 了6h的氧所氛处理;用扫描电镜和比表面测定对催化剂进行了表征;考察了催化剂对CO氧化反应的催化活性。结果表明,在CuMn1.36Ox中掺入稀土元素Ce大大增加了催化剂的比表面,Au在催化剂表面的分散度越高其活性越好,氧气氛  相似文献   

4.
弓风莲  代西民 《河南科学》1999,17(3):323-327
随着印染技术的发展,其生产工艺有很大改进,同时更多的化学印染助剂与化工原料广泛的应用于印染生产中,导致印染废水成份日趋复杂,对其治理难度增大。本文通过对技术更新前后的印染废水中CODMn与CODCr测定相关性研究结果表明:(1)印染废水中可生化性有机物成份呈下降趋势;(2)CODMn测定值越接近CODCr测定值时,废水中可生化物成分增大,与传统的BOD5与CODCr相关性研究结论相一致;(3)依据  相似文献   

5.
基于碘量法测定高温超导氧化物氧含量的方法,总结出固溶化合物Sm1+xBa2-xCu3On的氧含量n随固溶度x变化的规律性,从理论分析和实验测定得出在固溶区域内,Sm^1+xBa2-xCu3On的氧含量n与替代程序x呈线性关系,超出固溶极限x0,直线斜率将发生明显变化。此结果与X射线粉末衍射结果基本一致。  相似文献   

6.
以杂多酸H3PW12-nMonO40·xH2O(n=1,3)和三聚苯胺H2N-N-N-NH2为原料制备了钼磷杂多酸/三聚苯胺掺杂材料,用元素分析、红外光谱、紫外-可见光谱、X射线粉末射谱、热重分析等对此材料进行了表征,测定了其在不同有机溶剂(DMF,NMP〈CHCl3)中的溶解度,材料的荧光光谱表明,在366nm和863nm 处均有较好的荧光发射峰。  相似文献   

7.
氧化铈对Cu-Mn-O燃烧催化剂氧化还原性能的影响   总被引:1,自引:0,他引:1  
利用微反-色谱技术考察了Cu-Mn-O及Cu-Mn-Ce-O催化剂的甲苯完全燃烧活性;通过改变氧的浓度,研究了CeO_2对Cu-Mn-O催化剂性能的影响;用TPR、TPOT和氢氧滴定法测定了催化剂的表面性能。结果表明,CeO_2能够增加催化剂表面的贮氧量,提高吸氧能力,改进供氧性能,进而提高Cu-Mn-O催化剂在低氧比时的无化活性,也能使还原后的Cu-Mn-O催化剂具有良好的再生氧化活性。  相似文献   

8.
基于碘量法测定高温超导氧化物氧含量的方法,总结出固溶化合物Sm(1+x)Ba(2-x)Cu3On的氧含量n随固溶度x变化的规律性;从理论分析和实验测定得出在固溶区域内,Sm(1+x)Ba(2-x)Cu3On的氧含量n与替代程度x呈线性关系,超出固溶极限x0,直线斜率将发生明显变化。此结果与X射线粉末衍射结果基本一致.  相似文献   

9.
板栗中某些微量元素的测定及其营养研究   总被引:6,自引:0,他引:6  
对9种板栗测定了Cu,Zn,Mn含量.回收率在99.2%~108%之间.9个样品的Cu,Mn,Zn含量有差异.并且进行了样品中Cu,Mn,Zn含量的营养评价  相似文献   

10.
研究了直流等离子体原子发射光谱法同时测定人发中的Zn,Mn,Cu,Fe,Ca。讨论了Ca和Mg对Zn,Mn,Cu,Fe的干扰及对干扰的校正方法。对GBW09101进行了测定,结果与标准值吻合很好。对发样进行了实测和回收实验。Zn,Mn,Cu,Fe,Ca的回收率分别为92.9%~109%,92.0%~106%,94.0%~106%,94.0%~112%,89.3%~113%。  相似文献   

11.
There are numerous geometric objects stored in the spatial databases. An importance function in a spatial database is that users can browse the geometric objects as a map efficiently. Thus the spatial database should display the geometric objects users concern about swiftly onto the display window. This process includes two operations:retrieve data from database and then draw them onto screen. Accordingly, to improve the efficiency, we should try to reduce time of both retrieving object and displaying them. The former can be achieved with the aid of spatial index such as R-tree, the latter require to simplify the objects. Simplification means that objects are shown with sufficient but not with unnecessary detail which depend on the scale of browse. So the major problem is how to retrieve data at different detail level efficiently. This paper introduces the implementation of a multi-scale index in the spatial database SISP (Spatial Information Shared Platform) which is generalized from R-tree. The difference between the generalization and the R-tree lies on two facets: One is that every node and geometric object in the generalization is assigned with a importance value which denote the importance of them, and every vertex in the objects are assigned with a importance value,too. The importance value can be use to decide which data should be retrieve from disk in a query. The other difference is that geometric objects in the generalization are divided into one or more sub-blocks, and vertexes are total ordered by their importance value. With the help of the generalized R-tree, one can easily retrieve data at different detail levels.Some experiments are performed on real-life data to evaluate the performance of solutions that separately use normal spatial index and multi-scale spatial index. The results show that the solution using multi-scale index in SISP is satisfying.  相似文献   

12.
The discovery of the prolific Ordovician Red River reservoirs in 1995 in southeastern Saskatchewan was the catalyst for extensive exploration activity which resulted in the discovery of more than 15 new Red River pools. The best yields of Red River production to date have been from dolomite reservoirs. Understanding the processes of dolomitization is, therefore, crucial for the prediction of the connectivity, spatial distribution and heterogeneity of dolomite reservoirs.The Red River reservoirs in the Midale area consist of 3~4 thin dolomitized zones, with a total thickness of about 20 m, which occur at the top of the Yeoman Formation. Two types of replacement dolomite were recognized in the Red River reservoir: dolomitized burrow infills and dolomitized host matrix. The spatial distribution of dolomite suggests that burrowing organisms played an important role in facilitating the fluid flow in the backfilled sediments. This resulted in penecontemporaneous dolomitization of burrow infills by normal seawater. The dolomite in the host matrix is interpreted as having occurred at shallow burial by evaporitic seawater during precipitation of Lake Almar anhydrite that immediately overlies the Yeoman Formation. However, the low δ18O values of dolomited burrow infills (-5.9‰~ -7.8‰, PDB) and matrix dolomites (-6.6‰~ -8.1‰, avg. -7.4‰ PDB) compared to the estimated values for the late Ordovician marine dolomite could be attributed to modification and alteration of dolomite at higher temperatures during deeper burial, which could also be responsible for its 87Sr/86Sr ratios (0.7084~0.7088) that are higher than suggested for the late Ordovician seawaters (0.7078~0.7080). The trace amounts of saddle dolomite cement in the Red River carbonates are probably related to "cannibalization" of earlier replacement dolomite during the chemical compaction.  相似文献   

13.
AcomputergeneratorforrandomlylayeredstructuresYUJia shun1,2,HEZhen hua2(1.TheInstituteofGeologicalandNuclearSciences,NewZealand;2.StateKeyLaboratoryofOilandGasReservoirGeologyandExploitation,ChengduUniversityofTechnology,China)Abstract:Analgorithmisintrod…  相似文献   

14.
Instead of following Fock’s expansion,we solve the Schrodinger equation for some quantum mechanical manybody systems such as electrons in atoms and charged excitons in quantum wells in a similar way in hyperspherical coordinates by expanding the wave functions into orthonormal complete basis sets of the hyperspherical hannonics(HHs)of hyperangles and generalized Laguerre polynomials(GLPs)of the hyperradius.This leads the equation to  相似文献   

15.
Future mobile communication systems aim at providing very high data transmission rates, even in high-mobility scenarios such as high-speed wheel-track trains, maglev trains, highway vehicles, airplanes, guided missiles or spacecraft. A particularly important commercial application is the strong and increasing worldwide demand for high- speed broadband wireless communications (up to 574.8 km/ h test speeds or 380 km/h commercial speeds) in railways, providing data, voice and video services for applications such as onboard entertainment services to passengers, train control, train dispatch, train sensor status handling and sur- veillance. In such high-mobility scenarios, there are a number of communication challenges, including fast hand- over, location updating, high-speed channel modeling, estimation and equalization, anti-Doppler spreading tech- niques, fast power control, and dedicated network architec- ture. Because signal transmission in very high-speed scenarios will inevitably experience serious deterioration, it is imperative to develop key broadband mobile communi- cation techniques for such high-speed vehicles.  相似文献   

16.
17.
本文叙述了对海南岛及其毗邻大陆边缘白垩纪到第四纪地层岩石进行古地磁研究的全部工作过程。通过分析岩石中剩余磁矢量的磁偏角及磁倾角的变化,提出海南岛白垩纪以来经历的构造演化模式如下:早期伴随顺时针旋转而向南迁移,后期伴随逆时针转动并向北运移。联系该地区及邻区的地质、地球物理资料,对海南岛上述的构造地体运动提出以下认识:北部湾内早期有一拉张作用,主要是该作用使湾内地壳显著伸长减薄,形成北部湾盆地。从而导致了海南岛的早期构造运动,而海南岛后期的构造运动则主要是受南海海底扩张的影响。海南地体运动规律的阐明对于了解北部湾油气盆地的形成演化有重要的理论和实际意义。  相似文献   

18.
Being the primary media of geographical information and the elementary objects manipulated, almost all of maps adopt the layer-based model to represent geographic information in the existent GIS. However, it is difficult to extend the map represented in layer-based model. Furthermore, in Web-Based GIS, It is slow to transmit the spatial data for map viewing. In this paper, for solving the questions above, we have proposed a new method for representing the spatial data. That is scale-based model. In this model we represent maps in three levels: scale-view, block, and spatial object, and organize the maps in a set of map layers, named Scale-View, which associates some given scales.Lastly, a prototype Web-Based GIS using the proposed spatial data representation is described briefly.  相似文献   

19.
Various applications relevant to the exciton dynamics,such as the organic solar cell,the large-area organic light-emitting diodes and the thermoelectricity,are operating under temperature gradient.The potential abnormal behavior of the exicton dynamics driven by the temperature difference may affect the efficiency and performance of the corresponding devices.In the above situations,the exciton dynamics under temperature difference is mixed with  相似文献   

20.
The elongation method,originally proposed by Imamura was further developed for many years in our group.As a method towards O(N)with high efficiency and high accuracy for any dimensional systems.This treatment designed for one-dimensional(ID)polymers is now available for three-dimensional(3D)systems,but geometry optimization is now possible only for 1D-systems.As an approach toward post-Hartree-Fock,it was also extended to  相似文献   

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