涤纶织物氯化亚锡拔染印花工艺的研究(摘要)

由于涤纶是疏水性纤维，结构本身紧密，涤纶织物经高温高压染底色后采用氯化亚锡拔染印花必须借助于特殊的拔染印花助剂。本文研究了新拔染助剂WT－DA、有机酸、吸酸剂以及金属离子掩蔽剂对氯化亚锡拔染印花效果的影响，确定了各助剂的用量，并优化了汽蒸工艺条件，筛选了部分底色分散染料和着色染料。研究结果为：氯化亚锡拔染印花色浆由8份SnCI。，10～16份WT—DA，0．6份酒石酸，1～2份尿素，0．6～1份Na。SIO。和x份染料；印花后的汽蒸条件为190～200℃下汽蒸8～12min，相对湿度60％～70％；在此印花条件下，有9只底色染料和10只着色染料可用于拔染印花，拔染白度最高可达80％以上。     

苯骈噻吩酮衍生物甲川型分散染料的研究 染料分子结构与颜色的关系

本文对一系列不同结构的苯骈噻吩酮衍生物甲川型分散染料的染色涤纶进行了颜 色测量；研究了染料在涤纶上的颜色与染科分子结构的关系。     

分散染料的生物降解性能

采用了[BOD5]／[CODcr]和呼吸速率曲线两种方法对6大类14种分散染料的好氧生物降解性能进行测试。实验表明，分散染料在好氧状态下大都难降解。然后又考察了这些染料的厌氧生物降解性能，发现这些染料经厌氧反应后大都变得可生化降解，并且染料结构与其降解性能之间有一定的关系。     

臭氧脱色染浴中助剂的循环利用初探

通过分散染料和弱酸性染料的循环染色实验，筛选了几种在对染液通入臭氧后在氧化脱色条件下稳定的染色助剂，目的是为了减少臭氧脱色后的染液循环染色中助剂的用量，还研究了染浴臭氧脱色的工艺条件。     

涤纶织物氯化亚锡拔染印花工艺的研究

研究了新拔染助剂ＷＴ－ＤＡ在涤纶织物氯化亚锡拔染印花上的应用工艺，确定了氯化亚锡和各种助剂的最佳用量范围，优化了汽蒸工艺条件．并筛选了部分底色分散染料和着色分散染料。研究结果表明，涤纶织物氯化亚锡拔染印花是可行的，拔染白度，着色鲜艳度及花型精细度均可达到要求。     

活性污泥法处理印染废水中的主要微生物种群

对用活性污泥法处理印染废水中的微生物区系进行分离与鉴定，细菌与原生动物占优势．分离的２７０余株细菌大多数是具有芽孢、荚膜的革兰氏阳性杆菌．实验表明，分离的细菌对所用的分散染料的降解能力比活性染料强．凝结芽孢杆菌、枯草芽孢杆菌对两类染料都具有较强的降解活性；浸麻芽孢杆菌、坚实芽孢杆菌只对分散染料表现出较高的降解活性     

还原染料纱线染色中变性剂AC的应用

采用不同浓度变性剂ＡＣ与多种还原性染料在棉纱线染色中进行了缓染、匀染、移染分析对比实验,证明其对大多数还原性染料具有良好的匀染作用,有利于改善染色效果．     

2-氨基-3-氰基-4-氯-5-醛基噻吩类分散染料研究

合成了一系列以2—氨基—3—氰基—4—氯—5—醛基噻吩为重氮组分的分散染料，通过红外光谱、核磁共振谱、质谱等手段确证了所合成染料的结构．研究了染料的可见吸收光谱与染料结构之间的关系．测试了染料在涤纶上的牢度，该类染料水洗和摩擦牢度为4—5级，升华牢度在2—5级．     

用溶解度参数进行单偶氮分散染料的分子设计和结构筛选

本文提出了单偶氮分散染料溶解度参数的计算方法。分散染料的溶解度参数是染料结构决定染色性能的一个重要因素。有使用价值的分散染料其溶解度参数应和涤纶纤维溶解度参数相近,但这仅是必要条件,而不是充分条件。根据染料的溶解度参数,可以进行单偶氮分散染料的分子设计和初步筛选。     

三甲基四氢喹啉型杂环染料的研究 Ⅱ.甲川型分散染料的合成及结构与颜色关系

合成了２，２，４．７－四甲基－１．２，３，４－四氢喹啉的Ｎ－羟乙基，Ｎ－氯乙基，Ｎ－乙基 衍生物。由这些衍生物出发．合成了１０个四氢喹啉甲川型分散染料。讨论了染料的 结构与吸收光谱之间的关系，发现染料的摩尔消光系数较高，但四氢喹啉的７－位上 引入甲基后，摩尔消光系数有所下降；在环己烷中染料的最高吸收波长最小，摩尔 消光系数最大；在环己烷、丙酮、氯仿、乙醇、甲苯５种溶剂中，λｍａｘ与ζｍａｘ均呈 线性关系，经 ＰＰＰ－ＭＯ计算，染料 λｍａｘ的计算值与实验值基本一致。     

Characterization of Ordovician carbonate reservoirs, southeastern Saskatchewan, Canada

The discovery of the prolific Ordovician Red River reservoirs in 1995 in southeastern Saskatchewan was the catalyst for extensive exploration activity which resulted in the discovery of more than 15 new Red River pools. The best yields of Red River production to date have been from dolomite reservoirs. Understanding the processes of dolomitization is, therefore, crucial for the prediction of the connectivity, spatial distribution and heterogeneity of dolomite reservoirs.The Red River reservoirs in the Midale area consist of 3～4 thin dolomitized zones, with a total thickness of about 20 m, which occur at the top of the Yeoman Formation. Two types of replacement dolomite were recognized in the Red River reservoir: dolomitized burrow infills and dolomitized host matrix. The spatial distribution of dolomite suggests that burrowing organisms played an important role in facilitating the fluid flow in the backfilled sediments. This resulted in penecontemporaneous dolomitization of burrow infills by normal seawater. The dolomite in the host matrix is interpreted as having occurred at shallow burial by evaporitic seawater during precipitation of Lake Almar anhydrite that immediately overlies the Yeoman Formation. However, the low δ18O values of dolomited burrow infills (-5.9‰～ -7.8‰, PDB) and matrix dolomites (-6.6‰～ -8.1‰, avg. -7.4‰ PDB) compared to the estimated values for the late Ordovician marine dolomite could be attributed to modification and alteration of dolomite at higher temperatures during deeper burial, which could also be responsible for its 87Sr/86Sr ratios (0.7084～0.7088) that are higher than suggested for the late Ordovician seawaters (0.7078～0.7080). The trace amounts of saddle dolomite cement in the Red River carbonates are probably related to "cannibalization" of earlier replacement dolomite during the chemical compaction.     

An Index mechanism for multi-scale view in spatial databases

There are numerous geometric objects stored in the spatial databases. An importance function in a spatial database is that users can browse the geometric objects as a map efficiently. Thus the spatial database should display the geometric objects users concern about swiftly onto the display window. This process includes two operations:retrieve data from database and then draw them onto screen. Accordingly, to improve the efficiency, we should try to reduce time of both retrieving object and displaying them. The former can be achieved with the aid of spatial index such as R-tree, the latter require to simplify the objects. Simplification means that objects are shown with sufficient but not with unnecessary detail which depend on the scale of browse. So the major problem is how to retrieve data at different detail level efficiently. This paper introduces the implementation of a multi-scale index in the spatial database SISP (Spatial Information Shared Platform) which is generalized from R-tree. The difference between the generalization and the R-tree lies on two facets: One is that every node and geometric object in the generalization is assigned with a importance value which denote the importance of them, and every vertex in the objects are assigned with a importance value,too. The importance value can be use to decide which data should be retrieve from disk in a query. The other difference is that geometric objects in the generalization are divided into one or more sub-blocks, and vertexes are total ordered by their importance value. With the help of the generalized R-tree, one can easily retrieve data at different detail levels.Some experiments are performed on real-life data to evaluate the performance of solutions that separately use normal spatial index and multi-scale spatial index. The results show that the solution using multi-scale index in SISP is satisfying.     

A computer generator for randomly layered structures

AcomputergeneratorforrandomlylayeredstructuresYUJia shun1,2,HEZhen hua2(1.TheInstituteofGeologicalandNuclearSciences,NewZealand;2.StateKeyLaboratoryofOilandGasReservoirGeologyandExploitation,ChengduUniversityofTechnology,China)Abstract:Analgorithmisintrod…     

海南岛地体及其毗邻陆缘晚中生代—新生代古地磁研究和构造演化

本文叙述了对海南岛及其毗邻大陆边缘白垩纪到第四纪地层岩石进行古地磁研究的全部工作过程。通过分析岩石中剩余磁矢量的磁偏角及磁倾角的变化,提出海南岛白垩纪以来经历的构造演化模式如下:早期伴随顺时针旋转而向南迁移,后期伴随逆时针转动并向北运移。联系该地区及邻区的地质、地球物理资料,对海南岛上述的构造地体运动提出以下认识:北部湾内早期有一拉张作用,主要是该作用使湾内地壳显著伸长减薄,形成北部湾盆地。从而导致了海南岛的早期构造运动,而海南岛后期的构造运动则主要是受南海海底扩张的影响。海南地体运动规律的阐明对于了解北部湾油气盆地的形成演化有重要的理论和实际意义。     

Exciton Seebeck in Molecular Systems

Various applications relevant to the exciton dynamics,such as the organic solar cell,the large-area organic light-emitting diodes and the thermoelectricity,are operating under temperature gradient.The potential abnormal behavior of the exicton dynamics driven by the temperature difference may affect the efficiency and performance of the corresponding devices.In the above situations,the exciton dynamics under temperature difference is mixed with     

Achieving Unusual States of Matter Under High Pressure

The elongation method,originally proposed by Imamura was further developed for many years in our group.As a method towards O(N)with high efficiency and high accuracy for any dimensional systems.This treatment designed for one-dimensional(ID)polymers is now available for three-dimensional(3D)systems,but geometry optimization is now possible only for 1D-systems.As an approach toward post-Hartree-Fock,it was also extended to     

《Chinese Science Bulletin》SUBJECT INDEX TO VOLUME 59(2014)

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An on-line scaling method for improving scalability of a database cluster

The explosive growth of the Internet and database applications has driven database to be more scalable and available, and able to support on-line scaling without interrupting service. To support more client's queries without downtime and degrading the response time, more nodes have to be scaled up while the database is running. This paper presents the overview of scalable and available database that satisfies the above characteristics. And we propose a novel on-line scaling method. Our method improves the existing on-line scaling method for fast response time and higher throughputs. Our proposed method reduces unnecessary network use, i.e. , we decrease the number of data copy by reusing the backup data. Also, our on-line scaling operation can be processed parallel by selecting adequate nodes as new node. Our performance study shows that our method results in significant reduction in data copy time.     

An improved R-tree based on childnode''s probability

R-Tree is a good structure for spatial searching. But in this indexing structure,either the sequence of nodes in the same level or sequence of traveling these nodes when queries are made is random. Since the possibility that the object appears in different MBR which have the same parents node is different, if we make the subnode who has the most possibility be traveled first, the time cost will be decreased in most of the cases. In some case, the possibility of a point belong to a rectangle will shows direct proportion with the size of the rectangle. But this conclusion is based on an assumption that the objects are symmetrically distributing in the area and this assumption is not always coming into existence. Now we found a more direct parameter to scale the possibility and made a little change on the structure of R-tree, to increase the possibility of founding the satisfying answer in the front sub trees. We names this structure probability based arranged R-tree (PBAR-tree).     

Integrating GIS Web services based on mediating architecture

The geographic information service is enabled by the advancements in general Web service technology and the focused efforts of the OGC in defining XML-based Web GIS service. Based on these models, this paper addresses the issue of services chaining,the process of combining or pipelining results from several interoperable GIS Web Services to create a customized solution. This paper presents a mediated chaining architecture in which a specific service takes responsibility for performing the process that describes a service chain. We designed the Spatial Information Process Language (SIPL) for dynamic modeling and describing the service chain, also a prototype of the Spatial Information Process Execution Engine (SIPEE) is implemented for executing processes written in SIPL. Discussion of measures to improve the functionality and performance of such system will be included.