| 氧化锌棒晶的热液制备与表征 |
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| 引用本文： | 张艳辉,田彦文,邵忠财,钱建华. 氧化锌棒晶的热液制备与表征[J]. 东北大学学报(自然科学版), 2005, 26(11): 79-81. DOI: - |
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| 作者姓名： | 张艳辉 田彦文 邵忠财 钱建华 |
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| 作者单位： | 东北大学,材料与冶金学院,辽宁,沈阳,110004;沈阳理工大学,环境与化学工程学院,辽宁,沈阳,110168;渤海大学,化学化工学院,辽宁,锦州,121000 |
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| 摘 要： | 以二水醋酸锌、氢氧化钠为原料,长链聚乙二醇(PEG-20000)、环己烷为添加剂,制备出氧化锌微晶粉体.采用X射线衍射,扫描电镜和透射电镜等分析手段对粉体进行了表征.实验结果表明,在热液环境中,利用长链PEG不仅可以制备特殊形貌的氧化锌,也可以在环己烷的作用下,制备出大长径比的一维氧化锌棒.
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| 关 键 词： | 氧化锌 棒晶 PEG 环己烷 水热法 |
| 文章编号： | 1005-3026（2005）11-1096-03 |
| 收稿时间： | 2005-01-14 |
| 修稿时间： | 2005-01-14 |
Hydrothermal Synthesis and Characterization of ZnO Rod-Like Crystal |
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| ZHANG Yan-hui,TIAN Yan-wen,SHAO Zhong-cai,QIAN Jian-hua. Hydrothermal Synthesis and Characterization of ZnO Rod-Like Crystal[J]. Journal of Northeastern University(Natural Science), 2005, 26(11): 79-81. DOI: - |
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| Authors: | ZHANG Yan-hui TIAN Yan-wen SHAO Zhong-cai QIAN Jian-hua |
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| Affiliation: | (1) School of Materials and Metallurgy, Northeastern University, Shenyang 110004, China; (2) Faculty of Environment and Chemical Engineering, Shenyang Ligong University, Shenyang 110168, China; (3) Faculty of Chemistry and Chemical Engineering, Bohai University, Jinzhou 121000, China |
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| Abstract: | Zn(Ac)2 · 2H2O and NaOH were used as experimental material to synthesize ZnO microcrystal powder with long-chain PEG and cyclohexane as additives. XRD, SEM and TEM were used to characterize the powder. The experimental results showed that not only the special shape of ZnO was produced under the action of long-chain PEG, but also the one-dimension of rod-like ZnO with big aspect ratio can also be produced under the action of cyclohexane. |
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| Keywords: | PEG |
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