| 超声-微波协同萃取-HPLC检测掺罂粟壳肉汤中的生物碱 |
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| 引用本文： | 冯丽娟,王庭欣,赵志磊,孟玉彩,赵文,王继坤. 超声-微波协同萃取-HPLC检测掺罂粟壳肉汤中的生物碱[J]. 河北大学学报(自然科学版), 2009, 29(3): 291. DOI: 10.3969/j.issn.1000-1565.2009.03.016 |
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| 作者姓名： | 冯丽娟 王庭欣 赵志磊 孟玉彩 赵文 王继坤 |
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| 作者单位： | 1.河北农业大学,食品科技学院,河北,保定071001； 2.河北大学,质量技术监督学院,河北,保定071002； 3.北京中防昊通防伪科技中心,北京,100025 |
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| 摘 要： | 为建立食品中可能出现的罂粟壳生物碱成分--吗啡、可待因、罂粟碱的提取和测定方法,用超声-微波协同萃取的方法提取罂粟壳中的生物碱,高效液相色谱法(HPLC)进行含量分析.其平均回收率分别为97.87%,96.80%,94.47%;精密度相对标准偏差(RSD)分别为0.070%,0.037%,0.029%;重现性相对标准偏差(RSD)分别为0.040%,0.209%,0.665%.本方法具有回收率高、灵敏度高、精密度高等优点,可适用于食品中罂粟壳生物碱的检测.
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| 关 键 词： | 超声-微波协同萃取 高效液相色谱 罂粟壳生物碱 |
Determination of the Alkaloid in Food Added Opium Poppy Husk by Ultrasonic-microwave Synergistic Extraction-HPLC |
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| FENG Li-juan,WANG Ting-xin,ZHAO Zhi-lei,MENG Yu-cai,ZHAO Wen,WANG Ji-kun. Determination of the Alkaloid in Food Added Opium Poppy Husk by Ultrasonic-microwave Synergistic Extraction-HPLC[J]. Journal of Hebei University (Natural Science Edition), 2009, 29(3): 291. DOI: 10.3969/j.issn.1000-1565.2009.03.016 |
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| Authors: | FENG Li-juan WANG Ting-xin ZHAO Zhi-lei MENG Yu-cai ZHAO Wen WANG Ji-kun |
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| Abstract: | A method for the extraction and determination of morphine,codeine and papaverine in opium poppy husk probably added in foods was developed.The alkaloid in opium poppy husk were extracted by ultrasonic-microwave synergistic extraction technique and determined by high performance liquid chromatography(HPLC).The average recovery are 97.87%,96.80%,94.47% and the RSD of the precision are 0.070%,0.037%,0.029% and the RSD of the reproducibility are 0.040%,0.209%,0.665%,respectively.The method had high recovery,sensitivity and precision,that is suitable for the determination of the alkaloid in opium poppy husk in food. |
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| Keywords: | ultrasonic-microwave synergistic extraction HPLC alkaloid in opium poppy husk |
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