| 3—羟基—1,5—二氮杂环庚烷的合成研究 |
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| 引用本文： | 刘全忠 秦大斌. 3—羟基—1,5—二氮杂环庚烷的合成研究[J]. 西华师范大学学报(哲学社会科学版), 2000, 21(3): 255-256 |
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| 作者姓名： | 刘全忠 秦大斌 |
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| 作者单位： | 四川师范学院化学系!四川南充637002 |
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| 摘 要： | 对３－羟基－１，５－二氮杂环庚烷的合成进行了改进，在成环反应中以非离子溶剂代替了质子溶剂，缩短了反应时间、产率较文献有较大提高。
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| 关 键 词： | 合成 二氮杂环庚烷 非质子溶剂 |
Studies for the synthesis of 3-Hydroxyl-1,5-Dioazo-Cycloheptane |
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| LIU Quan zhong,QIN Da bin,JIANG Xiao hui. Studies for the synthesis of 3-Hydroxyl-1,5-Dioazo-Cycloheptane[J]. Journal of China West Normal University:Natural Science Edition, 2000, 21(3): 255-256 |
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| Authors: | LIU Quan zhong QIN Da bin JIANG Xiao hui |
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| Abstract: | An improvement was made on the synthesis of 3-hydroxyl-1,5-diazo-cycloheptane. In the process of cyclisation of the compound, the aprotic solvent was used by place of the protic one, thereby, the reaction time was shortened and the yield was higher than that reported in the literature. |
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| Keywords: | synthesis 3-hydroxyl-1 5-diazo-cycloheptane aprotic solvent. |
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