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化学发光法测定蜂蜜中金霉素残留含量
引用本文:付有利,章建军,贾艳,朱海华,李向力. 化学发光法测定蜂蜜中金霉素残留含量[J]. 河南科学, 2011, 29(10): 1178-1180
作者姓名:付有利  章建军  贾艳  朱海华  李向力
作者单位:1. 河南省商业科学研究所有限责任公司,郑州,450002
2. 河南省食品质量安全控制工程技术研究中心,郑州,450002
基金项目:郑州市2010年科技攻关项目(10PTGS504)
摘    要:采用化学发光法对蜂蜜中金霉素残留含量进行测定.结果:NaIO4为0.05 mol/L,H2O2为0.03 mol/L时,相对发光值△I与金霉素在相对低浓度0~8×10-7 g/mL和相对高浓度10×10-7~100×10-7g/mL范围内呈良好线性关系,相对标准偏差为2.12%,平均回收率为96.2%和97.6%.该法...

关 键 词:化学发光法  金霉素  蜂蜜

Determination on Chlortetracycline Residues in Honey by Chemiluminescence Analysis
Fu Youli,Zhang Jianjun,Jia Yan,Zhu Haihua,Li Xiangli. Determination on Chlortetracycline Residues in Honey by Chemiluminescence Analysis[J]. Henan Science, 2011, 29(10): 1178-1180
Authors:Fu Youli  Zhang Jianjun  Jia Yan  Zhu Haihua  Li Xiangli
Affiliation:Fu Youli,Zhang Jianjun,Jia Yan,Zhu Haihua,Li Xiangli (1.The Institute of food Commercial Sciences Co.,Ltd.,of Henan Province,Zhengzhou 450002,China,2.The Engineering Research Center of Food Quality and Safety Control of Henan Province,China)
Abstract:A method for determination on chlortetracycline residues in honey by chemiluminescence analysis.results :when the concentration of NaIO 4 was 0.05 mol/L,H 2 O 2 concentration of 0.03 mol/L,RLU and chlortetracycline at relatively low concentrations of 0~8×10-7 g /mL and a relatively high concentration of 10×10-7 ~100×10-7 g /mL range showed good linear relationship,the relative standard deviation is 2.12 %,the average recovery rate was 96.2 % and 97.6 %.This method is rapid,simple,accurate and reliable.
Keywords:chlortetracycline  chemiluminescence  honey  
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