| 室温离子液体中金纳米粒子的电化学制备及其表征 |
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| 引用本文： | 于爱风,陆文娟,王灿运,顾建胜. 室温离子液体中金纳米粒子的电化学制备及其表征[J]. 苏州大学学报(医学版), 2008, 24(2): 88-91 |
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| 作者姓名： | 于爱风 陆文娟 王灿运 顾建胜 |
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| 作者单位： | 苏州大学化学化工学院,江苏苏州215123 |
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| 基金项目： | 江苏省教育厅自然科学基金 |
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| 摘 要： | 室温离子液体1乙基3甲基咪唑四氟硼酸盐中,采用电化学牺牲阳极法直接从金属金制备了球形金纳米粒子，采用X射线衍射（XRD）、带有电子能谱仪（EDS）的扫描电子显微镜（SEM）对所制备样品的结构、组成以及形态进行了表征.结果表明,在本实验条件下制得的金纳米粒子为面心立方结构,纯度较高,基本呈球形,粒径平均尺寸为20nm.
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| 关 键 词： | 室温离子液体 电化学制备 金纳米粒子 |
| 文章编号： | 1000-2073(2008)02-0088-04 |
| 修稿时间： | 2008-01-09 |
Preparation and characterization of gold nanoparticles by electrochemical method in room temperature ionic liquid |
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| Yu Aifeng,Lu Wenjuan,Wang Canyun,Gu Jiansheng. Preparation and characterization of gold nanoparticles by electrochemical method in room temperature ionic liquid[J]. Journal of Suzhou University(Natural Science), 2008, 24(2): 88-91 |
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| Authors: | Yu Aifeng Lu Wenjuan Wang Canyun Gu Jiansheng |
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| Affiliation: | ( School of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215123 ) |
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| Abstract: | Spherical gold nanoparticles have been prepared by a sacrifice anode technique in a kind of room temperature ionic liquid,1-ethyl-3-methyl limidizaolium tetrafluoroborate（[emim]BF4）.The gold nanoparticles have been characterized by X-ray powder diffraction（XRD）and scan electron microscopy（SEM）with the energy dispersive spectroscopy（EDS）.Gold nanoparticles obtained under appropriate conditions possess face-centered cubic structure,high purity,sphericity and their average diameter was about 21nm. |
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| Keywords: | room temperature ionic liquid electrochemical synthesis gold nanoparticles |
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