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| TS-1分子筛合成与苯羟基化反应性能考察 | |
| 引用本文： | 戴延凤,刘希尧,萨学理,刘娟娟. TS-1分子筛合成与苯羟基化反应性能考察[J]. 江西科学, 1999, 17(4): 209-214 |
| 作者姓名： | 戴延凤 刘希尧 萨学理 刘娟娟 |
| 作者单位： | 1. 南昌大学化学系,江西南昌,330047 2. 北京燕山石油化工公司研究院,北京,102549 3. 北京石油化工科学研究院,北京,100083 |
| 基金项目： | 中国石化总公司1993 年度科研资助!课题《钛硅分子筛合成及应用》内容之一 |
| 摘 要： | 以TEOS、TBOT和自制的w =20 % TPAOH 水溶液为原料,合成了TS- 1 分子筛,并经IR、XRD和Raman 光谱等手段证实。用该分子筛作催化剂对芳烃羟基化催化性能进行考察,并在实验的基础上推测了TS- 1 分子筛催化芳烃直接羟基化的反应历程。 |
| 关 键 词： | TS-1分子筛 合成 芳烃 羟基化 |
Synthesis of Zeolite TS-1 and Its Catalysis Properties in Hydroxylation of Benzene to Phenol |
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| DAI Yan-feng,LIU Xi-yao,SA Xue-li,LIU Juan-juan. Synthesis of Zeolite TS-1 and Its Catalysis Properties in Hydroxylation of Benzene to Phenol[J]. Jiangxi Science, 1999, 17(4): 209-214 | |
| Authors: | DAI Yan-feng LIU Xi-yao SA Xue-li LIU Juan-juan |
| Abstract: | Zeolite TS-1 is prepared starting from a mixture constituted by TEOS,TBOT and TPAOH.The TS-1 is characterized by some methods such as IR,XRD and Raman spectrum etc.With TS-1 prepared as catalyst,the hydroxylation of benzene under mild conditions has been studied.Finally the mechanism of benzene hydroxylation is discussed. |
| Keywords: | TS-1 zeolites Synthesis Benzene Hydroxylation |
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