| 邻溴甲基苯甲酸的合成研究 |
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| 引用本文： | 王娟,杨云龙,王萍,刘福德.邻溴甲基苯甲酸的合成研究[J].天津理工大学学报,2011,27(3):73-75. |
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| 作者姓名： | 王娟 杨云龙 王萍 刘福德 |
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| 作者单位： | 天津理工大学化学化工学院,天津,300384 |
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| 摘 要： | 以邻甲基苯甲酸和溴为原料,分别采用AIBN引发和光引发自由基反应合成了邻溴甲基苯甲酸,并利用IR和1H NMR对所得产品进行表征.考察了原料配比、溶剂种类、反应时间和引发剂用量对反应的影响.
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| 关 键 词： | 邻甲基苯甲酸 溴化 自由基反应 邻溴甲基苯甲酸 |
Investigation on synthesis of 2-(bromomethyl) benzoic acid |
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| WANG Juan,YANG Yun-long,WANG Ping,LIU Fu-de.Investigation on synthesis of 2-(bromomethyl) benzoic acid[J].Journal of Tianjin University of Technology,2011,27(3):73-75. |
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| Authors: | WANG Juan YANG Yun-long WANG Ping LIU Fu-de |
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| Institution: | (School of Chemistry and Chemical Engineering,Tianjin University of Technology,Tianjin 300384,China) |
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| Abstract: | 2-(bromomethyl) benzoic acid was synthesized by using 2-methylbenzoic and bromine as the basic materials through free radical reaction under light or with AIBN as initiator.The product was characterized by IR and 1H NMR.The effects of the mole ratio of the materials,different solvents,reaction time and the amount of initiator on yield were investigated. |
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| Keywords: | 2-methylbenzoic bromination free radical reaction 2-(bromomethyl) benzoic acid |
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