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微波法制备立方相BaTiO3及其表征
引用本文:李军平,畅功民,郑娜,张智敏.微波法制备立方相BaTiO3及其表征[J].山西大学学报(自然科学版),2006,29(4):388-390.
作者姓名:李军平  畅功民  郑娜  张智敏
作者单位:1. 山西大学,化学化工学院,山西,太原,030006
2. 山西省农业科学院,山西,太原,030031
摘    要:采用微波法制备了纳米晶B aT iO3,并通过XRD、SEM、TG及原子吸收等对产物进行了表征.XRD分析表明晶体为立方相B aT iO3,SEM显示B aT iO3颗粒形貌主要为立方相,一次粒子的粒径约为50 nm,TG分析表明所制得的B aT iO3粉体晶形稳定,原子吸收分析表明所制得的B aT iO3粉体杂质总含量为0.0261%.

关 键 词:立方相  微波法  纳米晶
文章编号:0253-2395(2006)04-0388-03
收稿时间:2006-05-11
修稿时间:2006年5月11日

Preparation and Characterization of Cubic Phase Barium Titanate by Microwave Method
LI Jun-ping,CHANG Gong-min,ZHENG Na,ZHANG Zhi-min.Preparation and Characterization of Cubic Phase Barium Titanate by Microwave Method[J].Journal of Shanxi University (Natural Science Edition),2006,29(4):388-390.
Authors:LI Jun-ping  CHANG Gong-min  ZHENG Na  ZHANG Zhi-min
Institution:1. School of Chemistry and Chemical Engineering ,Shanxi University ,Taiyuan 030006 ,China 2. Shanxi Academy of Agricultural Sciences, Taiyuan 030031 ,China
Abstract:The nano-crystalline Barium Titanate was prepared by the microwave method.The morphological feature of the product was characterized by ways of XRD,SEM,TG and atomic absorption.The result showed that the crystal was cubic phase structure by XRD analysis and the first grade grain size was about 50 nm by SEM;the crystal form was stable using TG;the amount of impurity was about the percent of 0.0261 by the atomic absorption.
Keywords:BaTiO3
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