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半枝莲中黄酮成分的提取纯化及LC-MS检测
引用本文:王英锋,焦燕,王慧彬,郭雪清,李中峰.半枝莲中黄酮成分的提取纯化及LC-MS检测[J].首都师范大学学报(自然科学版),2009,30(5):32-34.
作者姓名:王英锋  焦燕  王慧彬  郭雪清  李中峰
作者单位:首都师范大学分析测试中心,北京,100048
摘    要:提取纯化半枝莲中的黄酮成分.方法:采用醇提法提取半枝莲中的黄酮成分,利用大孔树脂法分离纯化,运用液相色谱-质谱联用法(LC-MS)进行检测.结果:半枝莲黄酮成分主要存在于20%乙醇洗脱部分和40%乙醇洗脱部分.结论:结果说明此提取纯化方法具有可行性.

关 键 词:半枝莲  黄酮  提取  纯化  液相色谱-质谱.

Studies on the Flavonoids in Scutellaria barbata with LC-MS
Wang Yingfeng,Jiao Yan,Wang Huibin,Guo Xueqing,Li Zhongfeng.Studies on the Flavonoids in Scutellaria barbata with LC-MS[J].Journal of Capital Normal University(Natural Science Edition),2009,30(5):32-34.
Authors:Wang Yingfeng  Jiao Yan  Wang Huibin  Guo Xueqing  Li Zhongfeng
Institution:The Analysis Test Center of Capital Normal University;Beijing 100048
Abstract:to study the flavonoids in medicine Scutellaria barbata D.Don.Method:the flavonoids in the Scutellaria barbata D.Don were distilled by ethanol, sublimated by macroporous resin and analyzed by LC-MS.Results :the flavonoids were gotten from the parts desorbing with 20% and 40% ethanol.Conclusion:these methods of distillation and purification are doable.
Keywords:Scutellaria barbata D  Don  flavonoids  extract  sublimate  LC-MS    
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