| 续断片及其盐炙品高效液相指纹图谱 |
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| 引用本文： | 罗君,卿娟,张丽艳,张丽丽.续断片及其盐炙品高效液相指纹图谱[J].信阳师范学院学报(自然科学版),2015(2):235-238. |
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| 作者姓名： | 罗君 卿娟 张丽艳 张丽丽 |
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| 作者单位： | 贵阳中医学院第一附属医院;贵州省修文县疾病预防控制中心;贵阳中医学院 |
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| 基金项目： | 国家科技支撑项目(2009BA174B1-4);贵阳市科学技术计划项目([2010]筑科合同字第1-中-16号) |
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| 摘 要： | 采用Agilent C18色谱柱(4.6 mm×250 mm,5μm),流动相乙腈-0.05%磷酸水溶液梯度洗脱,流速1.0 m L·min-1,柱温25℃,建立了续断片和盐续断HPLC指纹图谱的测定方法,以川续断皂苷Ⅵ为参照峰,标定了29个共有峰.结果表明,该法重复性好,专属性强,可为续断片和盐续断饮片质量控制提供科学依据.
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| 关 键 词： | 续断 盐制 指纹图谱 |
HPLC Fingerprint Chromatograms of Dipsacus asper and Salt-processed |
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| Luo Jun;Qing Juan;Zhang Liyan;Zhang Lili.HPLC Fingerprint Chromatograms of Dipsacus asper and Salt-processed[J].Journal of Xinyang Teachers College(Natural Science Edition),2015(2):235-238. |
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| Authors: | Luo Jun;Qing Juan;Zhang Liyan;Zhang Lili |
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| Institution: | Luo Jun;Qing Juan;Zhang Liyan;Zhang Lili;The First Affiliated Hospital of Guiyang College of Traditional Chinese Medicine;Center for Disease Control and Prevention of Xiuwen City;Guiyang College of Traditional Chinese Medicine; |
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| Abstract: | The HPLC fingerprint chromatograms of Dipsacus asper and salt-processed was established on an Agilent C18( 4. 6 mm × 250 mm,5 μm) column with isocratic elution of acetonitrile-0. 05% phosphoric acid at a flow rate of1. 0 m L·min- 1and the column temperature of 25 ℃. There were 29 common peaks which referred to asperosaponinⅥ. The results showed that the method was repeatable,exclusive and could provide scientific basis for quality control of Gentiana rhodantha. |
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| Keywords: | Dipsacus asper salt-process fingerprint |
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