| 溶剂法醇解合成三甲氧基硅烷的研究 |
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| 引用本文： | 何军,刘运美.溶剂法醇解合成三甲氧基硅烷的研究[J].南华大学学报(自然科学版),2003,17(4):91-93. |
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| 作者姓名： | 何军 刘运美 |
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| 作者单位： | 1. 南华大学,化学化工学院,湖南,衡阳,421001
2. 南华大学,生命科学与技术学院,湖南,衡阳,421001 |
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| 摘 要： | 在改进的装置中采用溶剂法,以三氯硅烷和甲醇为原料醇解合成三甲氧基硅烷.通过考察溶剂种类、原料配比、冷凝温度、填料大小等因素的影响,确立了最优合成条件.
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| 关 键 词： | 三甲氧基硅烷 三氯硅烷 甲醇 |
| 文章编号： | 1006-737X(2003)04-0091-03 |
| 修稿时间： | 2003年9月26日 |
Alcoholysis Synthesis of Trimethoxysilane by Solution method |
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| HE Jun,LIU Yun-mei.Alcoholysis Synthesis of Trimethoxysilane by Solution method[J].Journal of Nanhua University:Science and Technology,2003,17(4):91-93. |
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| Authors: | HE Jun LIU Yun-mei |
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| Institution: | HE Jun~1 LIU Yun-mei~2 |
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| Abstract: | In the improved equipment, trimethoxysilane was synthesized with CH_3OH and HSiCl3 by solution method. The influence of reaction conditions such as solvent, ratio of material , temperature of cooling fluid , size of filling were observed. The optimum conditions for synthesizing trimethoxysilane were established. |
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| Keywords: | trimethoxysilane tricholorosilane methanol |
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