| 6，7-环氧柠檬醛的合成 |
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| 引用本文： | 尚利亚,杨始刚,陶建伟.6，7-环氧柠檬醛的合成[J].上海应用技术学院学报,2013,13(1):27-30. |
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| 作者姓名： | 尚利亚 杨始刚 陶建伟 |
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| 作者单位： | 上海应用技术学院化学与环境工程学院,上海,201418 |
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| 摘 要： | 以柠檬醛为原料,二氯甲烷为溶剂,反应温度0～10℃,间氯苯过甲酸与柠檬醛的物质的量之比为1.1∶1,反应8h,得6,7-环氧柠檬醛粗产物.产物经硅胶柱分离,用乙酸乙酯石油醚(体积比)=1:6作为洗脱剂,得到纯净的6,7-环氧柠檬醛,得率约为75.0％,产物经红外和核磁共振鉴定.
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| 关 键 词： | 柠檬醛 间氯苯过甲酸 6 7-环氧柠檬醛 洗脱剂 |
Synthesis of 6,7-Epoxycitral |
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| SHANG Li-y,YANG Shi-gang and TAO Jian-wii.Synthesis of 6,7-Epoxycitral[J].Journal of Shanghai Institute of Technology: Natural Science,2013,13(1):27-30. |
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| Authors: | SHANG Li-y YANG Shi-gang and TAO Jian-wii |
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| Institution: | School of Chemical and Environmental Engineering, Shanghai Institute of Technology, Shanghai 201418, China;School of Chemical and Environmental Engineering, Shanghai Institute of Technology, Shanghai 201418, China;School of Chemical and Environmental Engineering, Shanghai Institute of Technology, Shanghai 201418, China |
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