| Abstract: | The raw materials were commercial powders of Nb2O5 (99.95%),reactive carbon (99.99%),NaCl (99.95%) and sucrose (99.94%).By the carbothermal method,the NbCx (x= 0.98)-C composite three-dimensional netted fibers were prepared in graphite resistance furnace in 0.1 MPa/N2 ambient atmosphere at temperature from 970 to 1 120℃.The diameters of composite three-dimensional netted fibers are 12-38 m m,the hole circumferences of netted fibers are 0.22-2.2 mm,and the hole diameters are 70-701 m m.The process conditions for fabricating NbCx-C composite three-dimensional netted fibers and related morphology,composition and crystal structure of NbCx-C composite netted fibers were investigated in detail. |
