| 固体催化剂催化乙酸与正丁醇酯化反应产物的气相色谱分析 |
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| 引用本文： | 陈培丰,郑瑛.固体催化剂催化乙酸与正丁醇酯化反应产物的气相色谱分析[J].福建师范大学学报(自然科学版),1997,13(2):60-65. |
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| 作者姓名： | 陈培丰 郑瑛 |
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| 摘 要： | 分析了不同气相色谱固定相对乙酸与正丁醇酯化反应产物色谱分析的影响，用正交试验对色谱操作参数进行优化选择，在所选最佳色谱条件下对内标物进行筛选，实验结果表明，Ｃ ＧＤＸ－１０４为固定相，使用氢焰离子化检测器，环己酮为内标，在本实验所确定的郄谱条件下，分析结果符合定必和定量的要求，整个分析过程无需对样品进行化学预处理，快速、简捷、准确度高。
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| 关 键 词： | 乙酸 正丁醇 乙酸丁酯 气相色谱分析 酯化反应 |
The Analysis of the Esterification Products of Acetic Acid and Butanol |
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| Chen,Peifeng,Zheng,Ying,Wang,Shiming.The Analysis of the Esterification Products of Acetic Acid and Butanol[J].Journal of Fujian Teachers University(Natural Science),1997,13(2):60-65. |
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| Authors: | Chen Peifeng Zheng Ying Wang Shiming |
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| Institution: | Department of Chemistry |
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| Abstract: | A rapid GC method has been developed for separating a mixture of the esterification products of acetic acid and butanol.The experiment results show that the stainless steel column was contained GDX-104 and cyclohexanone was for the interior standard,the esterification products of acetic acid and butanol are analysed qualitatively and quantitatively. This method has the features of simplicity, rapidity and accuracy. |
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| Keywords: | acetic acid butanol n-butyl acetate cyclohexanone gas chromatography analysis |
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