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Ag/AgCl高温参比电极的制备
引用本文:张清,李萍,白真权.Ag/AgCl高温参比电极的制备[J].应用科技,2005,32(6):62-63.
作者姓名:张清  李萍  白真权
作者单位:1. 河南科技大学,材料科学与工程学院,河南,洛阳,471003
2. 洛阳工业高等专科学校,建筑工程系,河南,洛阳,471003
3. 中国石油天然气集团公司,石油管材研究所,陕西,西安,710065
基金项目:中国石油天然气集团公司石油管材研究所基金资助项目(23-524),河南科技大学科研基金资助项目(200101).
摘    要:在对美国Cortest公司设计的Ag/AgCl参比电极进行改进的基础上,采用电解法制备了一种内置式Ag/AgCl参比电极,对其进行了性能测试,并用其对油管钢N80的高温高压腐蚀行为多次进行了测试研究.结果表明,该参比电极具有重现性好、可逆性好、响应时间短、内阻小等优良性能,且在高温高压条件下工作性能稳定,测试曲线理想,可用于高温高压电化学研究.

关 键 词:Ag/AgCl参比电极  电解  制备
文章编号:1009-671X(2005)06-0062-02
修稿时间:2004年12月28

Preparation of an elevated temperature Ag/AgCl reference electrode
ZHANG Qing,LI Ping,BAI Zhen-quan.Preparation of an elevated temperature Ag/AgCl reference electrode[J].Applied Science and Technology,2005,32(6):62-63.
Authors:ZHANG Qing  LI Ping  BAI Zhen-quan
Institution:ZHANG Qing~1,LI Ping~2,BAI Zhen_quan~3
Abstract:On the basis of the improvement of Ag/AgCl reference electrode of Cortest Company in America, the internal Ag/AgCl reference electrodes were prepared by means of electrolyzing. Their features were tested and the corrosion behavior of tubular steel N80 under high temperature and high pressure were studied with them. The results show that it has such outstanding features as good reproducibility and reversibility, short response time and small resistance. The new electrodes worked stably and ideal test curves were obtained under high temperature and high pressure, and could be used in electrochemical research under high temperature and high pressure.
Keywords:Ag/AgCl reference electrode  electrolyzing  preparation
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