| 还原气化冷原子吸收光谱法测定“六味地黄丸”中痕量汞 |
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| 引用本文： | 覃事栋,姚俊,张永康,杨成隆,庄峙厦,王小如.还原气化冷原子吸收光谱法测定“六味地黄丸”中痕量汞[J].吉首大学学报(自然科学版),1996(3). |
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| 作者姓名： | 覃事栋 姚俊 张永康 杨成隆 庄峙厦 王小如 |
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| 作者单位： | 吉首大学化学系!湖南吉首,416000,吉首大学化学系!湖南吉首,416000,吉首大学化学系!湖南吉首,416000,厦门大学化学系!中国厦门,361005,厦门大学化学系!中国厦门,361005,厦门大学化学系!中国厦门,361005 |
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| 基金项目： | 国家教委重点实验室资助 |
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| 摘 要： | 本文采用自制电热恒温石英管还原气化冷原子吸收光谱法,直接测定了六味地黄丸中的痕量汞。方法检出限为0·1PPb;回收率为90～98％;相对标准偏差为4．3％。该方法简便,重现性好,准确度高。可用于中成药中痕量汞的测定。
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| 关 键 词： | 原子吸收光谱法 六味地黄丸 痕量汞 冷原子发生 |
Determination of Trace Mercury in Samples of "Liu Wei Di Huang Wan" by Cold-Atom Generation Atomic Spectrometry |
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| Qin Shidong ,Yao Jun ,Zhang Yongkang ,.Determination of Trace Mercury in Samples of "Liu Wei Di Huang Wan" by Cold-Atom Generation Atomic Spectrometry[J].Journal of Jishou University(Natural Science Edition),1996(3). |
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| Authors: | Qin Shidong Yao Jun Zhang Yongkang |
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| Abstract: | Using a homemade device of the electric heated quartz-tube atomizer,including a con-trolling temperature unit and a continue hydride generator,trace mercury in samples of "liuWei Di Huang Wan"has been determined directly. The method is simple,convenient, and ofgood precision and high accuracy. It is a very practical method for the analysis of trace mer-cury- The determination limit is below O. 1ppb,and the recovery is 90- 98%' |
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| Keywords: | AAS Trace Mercury Cold -atom generation Traditional Chinese medicine |
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