| HPLC测定平消胶囊中马钱子碱和仙鹤草酚的含量 |
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| 引用本文： | 周大祥,刘仁华.HPLC测定平消胶囊中马钱子碱和仙鹤草酚的含量[J].重庆三峡学院学报,2009,25(3):89-91. |
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| 作者姓名： | 周大祥 刘仁华 |
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| 作者单位： | 1. 重庆三峡学院生物系,重庆万州,404000
2. 三峡库区可持续发展研究中心,重庆万州,404000 |
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| 基金项目： | 重庆三峡学院院级项目《傅里叶变换红外光谱等分析平消胶囊有效成份》研究成果之一 |
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| 摘 要： | 为了测定抗胆管癌中成药平消胶囊的有效成分马钱子碱和仙鹤草酚的含量，本实验采用高效液相色谱法．结果发现马钱子碱在0．102～0．918μg、仙鹤草酚在0．01196～0．1125μg范围线性关系良好，相关系数分别为0．9999和0．9998；平均回收率分别为99．28％（RSD=1．65％）、101．04％（RSD=1．37％），平消胶囊中马钱子碱的含量为0．855mg／g，仙鹤草酚的含量为1．372mg／g．本方法操作可靠、精确，适用于平消胶囊中马钱子碱和仙鹤草酚的含量测定．
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| 关 键 词： | 平消胶囊 马钱子碱 仙鹤草酚 高效液相色谱法 |
Determination the Contents of Bruchine and Agrimophol in Pingxiao Capsule by HPLC |
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| Zhou Da-xiang,LIU Ren-hua.Determination the Contents of Bruchine and Agrimophol in Pingxiao Capsule by HPLC[J].JOurnal of Chongqing Three Gorges University,2009,25(3):89-91. |
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| Authors: | Zhou Da-xiang LIU Ren-hua |
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| Institution: | Department of Biology;Chongqing Three Gorges University;Wanzhou 404000;Chongqing;Research Center of Sustainable Development in Three Gorges Reservoir Area;Wanzhou 404000 |
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| Abstract: | To establish the HPLC method for determination of Bruchine and Agrimophol in Pingxiao capsule. Results find The linear ranage of Bruchine and Agrimophol were 0.102-0.918μg and 0.01196-0.1125μg respectively. The recovery rates of Bruchine and Agrimophol were 99.28% （RSD=1.65%） and 101.04% （RSD=1.37%） respectively. The content of Bruchine and Agrimophol is 0.855mg/g and 1.372mg/g in Pingxiao capsule. This method is realiable and accurate, the method can be applied to determination the contents of Bruchine and Agrimophol in Pingxiao capsule. |
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| Keywords: | Pingxiao capsule Bruchine Agrimophol HPLC |
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