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气相色谱-质谱法对柠檬酸三丁酯的检测研究
引用本文:姚李,吴缨. 气相色谱-质谱法对柠檬酸三丁酯的检测研究[J]. 合肥学院学报(自然科学版), 2008, 18(1): 49-51
作者姓名:姚李  吴缨
作者单位:合肥学院,化学与材料工程系,合肥,230022;合肥学院,化学与材料工程系,合肥,230022
摘    要:建立了GC—MS对柠檬酸三丁酯的定性与定量分析方法.全扫描方式定性,选择离子方式定量,外标法线性相关系数为0.994,方法回收率为91.0%~107.0%,相对标准偏差为5.23%~6.95%.

关 键 词:柠檬酸三丁酯  气相色谱-质谱  定量分析
文章编号:1673-162X(2008)01-0049-03
修稿时间:2007-09-06

Research on Tributyl Citrate by Gas Chromatography - Mass Spectrometry
YAO Li,WU Ying. Research on Tributyl Citrate by Gas Chromatography - Mass Spectrometry[J]. Journal of Hefei University(Natural Sciences Edition), 2008, 18(1): 49-51
Authors:YAO Li  WU Ying
Affiliation:(Department of Chemistry and Material Engineering, Hefei University,Hefei 230022, China)
Abstract:Qualitative and quantitative analysis of TBC is carried out by GC-MS. Scanning is selected for qualitative analysis and SIM for quantitative analysis. Results show that the linear coefficient is 0. 994 using external standard method. The recovery rate is 91.0% - 107.0% and the relative standard deviation is from 5.23% to 6.95% .
Keywords:TBC  Gas Chromatography-Mass Spectrometry  quantitative analysis
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